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MassMS-NW-7936 1,2-bis(2-(2-pyridyl)ethylthio)ethane C16H20N2S2 (Mass of molecular ion: 304)
Source Temperature: 180 °C Sample Temperature: 120 °C Direct, 75 eV
18.0 1.9 27.0 3.5 28.0 2.0 39.0 4.0 45.0 2.8 50.0 1.3 51.0 6.7 52.0 4.1 53.0 3.3 54.0 1.5 59.0 1.3 61.0 1.5 65.0 4.4 66.0 2.2 77.0 4.2 78.0 19.9 79.0 7.6 80.0 1.9 92.0 4.6 93.0 29.0 94.0 5.9 104.0 4.7 105.0 3.3 106.0 93.4 107.0 11.1 118.0 1.5 132.0 2.1 136.0 3.6 137.0 1.6 138.0 58.4 139.0 43.9 140.0 7.0 141.0 2.2 152.0 4.1 166.0 100.0 167.0 11.1 168.0 5.2 198.0 4.5 199.0 3.8
400 MHz in CDCl3
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1H NMR 399.65 MHz C16 H20 N2 S2 0.047 g : 0.5 ml CDCl3 1,2-bis(2-(2-pyridyl)ethylthio)ethane 
Assign. Shift(ppm)
A 8.538 B 7.603 C 7.177 D 7.131 E 3.059 F 2.964 G 2.716
Hz ppm Int.3416.26 8.549 82 3415.41 8.547 93 3414.55 8.544 94 3413.57 8.542 86 3411.38 8.536 85 3410.52 8.534 94 3409.67 8.532 92 3408.69 8.530 81 3047.49 7.626 71 3045.65 7.621 71 3039.79 7.607 139 3037.96 7.602 141 3032.10 7.587 86 3030.27 7.583 85 2872.31 7.188 140 2864.62 7.168 131 2856.81 7.149 80 2855.59 7.146 74 2851.93 7.137 83 2850.71 7.134 79 2849.24 7.130 81 2848.14 7.127 71 2844.36 7.118 75 2843.26 7.115 68 1231.45 3.082 76 1229.98 3.078 80 1223.27 3.061 185 1221.92 3.058 112 1215.70 3.042 190 1191.16 2.981 218 1190.31 2.979 211 1185.91 2.968 76 1184.81 2.965 144 1183.23 2.961 249 1182.01 2.958 174 1176.64 2.945 107 1175.05 2.941 95 1085.57 2.717 1000
in CDCl3
KBr disc
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