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网站主页CAS数据库列表 64691-70-9更多图谱1,8-双(2-吡啶基)-3,6-二硫杂辛烷(64691-70-9)核磁图(1HNMR)

1,8-双(2-吡啶基)-3,6-二硫杂辛烷

产品名称 1,8-双(2-吡啶基)-3,6-二硫杂辛烷

CAS号64691-70-9

分子式C16H20N2S2

分子量304.47


  • Mass

    MS-NW-7936          
    1,2-bis(2-(2-pyridyl)ethylthio)ethane
    C16H20N2S2          (Mass of molecular ion:    304)
    

       Source Temperature: 180 °C
       Sample Temperature: 120 °C
       Direct, 75 eV
    

          18.0       1.9
          27.0       3.5
          28.0       2.0
          39.0       4.0
          45.0       2.8
          50.0       1.3
          51.0       6.7
          52.0       4.1
          53.0       3.3
          54.0       1.5
          59.0       1.3
          61.0       1.5
          65.0       4.4
          66.0       2.2
          77.0       4.2
          78.0      19.9
          79.0       7.6
          80.0       1.9
          92.0       4.6
          93.0      29.0
          94.0       5.9
         104.0       4.7
         105.0       3.3
         106.0      93.4
         107.0      11.1
         118.0       1.5
         132.0       2.1
         136.0       3.6
         137.0       1.6
         138.0      58.4
         139.0      43.9
         140.0       7.0
         141.0       2.2
         152.0       4.1
         166.0     100.0
         167.0      11.1
         168.0       5.2
         198.0       4.5
         199.0       3.8
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C16 H20 N2 S2 0.047 g : 0.5 ml CDCl3
    1,2-bis(2-(2-pyridyl)ethylthio)ethane
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.538 B 7.603 C 7.177 D 7.131 E 3.059 F 2.964 G 2.716

         Hz     ppm     Int.
    

       3416.26   8.549     82
       3415.41   8.547     93
       3414.55   8.544     94
       3413.57   8.542     86
       3411.38   8.536     85
       3410.52   8.534     94
       3409.67   8.532     92
       3408.69   8.530     81
       3047.49   7.626     71
       3045.65   7.621     71
       3039.79   7.607    139
       3037.96   7.602    141
       3032.10   7.587     86
       3030.27   7.583     85
       2872.31   7.188    140
       2864.62   7.168    131
       2856.81   7.149     80
       2855.59   7.146     74
       2851.93   7.137     83
       2850.71   7.134     79
       2849.24   7.130     81
       2848.14   7.127     71
       2844.36   7.118     75
       2843.26   7.115     68
       1231.45   3.082     76
       1229.98   3.078     80
       1223.27   3.061    185
       1221.92   3.058    112
       1215.70   3.042    190
       1191.16   2.981    218
       1190.31   2.979    211
       1185.91   2.968     76
       1184.81   2.965    144
       1183.23   2.961    249
       1182.01   2.958    174
       1176.64   2.945    107
       1175.05   2.941     95
       1085.57   2.717   1000
    

in CDCl3



KBr disc



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