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网站主页CAS数据库列表 64501-87-7更多图谱N-(4-硝基苯磺酰)-L-苯丙氨酸(64501-87-7)质谱(MS)

N-(4-硝基苯磺酰)-L-苯丙氨酸

产品名称 N-(4-硝基苯磺酰)-L-苯丙氨酸

CAS号64501-87-7

分子式C15H14N2O6S

分子量350.35

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  • Mass

    MS-IW-5659          
    N-(p-nitrophenylsulfonyl)-L-phenylalanine
    C15H14N2O6S         (Mass of molecular ion:    350)
    

       Source Temperature: 180 °C
       Sample Temperature: 180 °C
       Direct, 75 eV
    

          18.0       3.1
          28.0       2.3
          39.0       1.9
          44.0       4.1
          50.0       2.7
          51.0       2.3
          63.0       1.7
          64.0       1.9
          65.0       7.6
          75.0       4.1
          76.0       5.6
          77.0       4.2
          89.0       2.0
          90.0       2.3
          91.0     100.0
          92.0      17.3
          93.0       1.4
         106.0       1.7
         117.0       4.9
         118.0      18.6
         119.0       7.8
         120.0       2.5
         122.0      12.9
         123.0       2.0
         147.0       3.3
         148.0      43.8
         149.0       4.6
         156.0       4.3
         163.0       2.0
         164.0       1.9
         186.0      11.6
         187.0       1.3
         204.0       5.0
         259.0       6.5
         304.0       3.0
         305.0       4.5
    

400 MHz in DMSO-d6


  • 1H NMR 399.65 MHz
    C15 H14 N2 O6 S 0.040 g : 0.5 ml DMSO-d6
    N-(p-nitrophenylsulfonyl)-L-phenylalanine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 12.9 B 8.75 C 8.209 D 7.758 E 7.13 F 3.983 G *1 3.004 J *1 2.731

         Hz     ppm     Int.
    

       5155.04  12.899     80
       3503.61   8.767    221
       3494.45   8.744    231
       3288.02   8.228     75
       3285.64   8.222    566
       3283.63   8.217    192
       3281.43   8.211     39
       3278.68   8.204    200
       3276.67   8.199    615
       3274.28   8.193     91
       3107.60   7.776     89
       3105.04   7.770    607
       3103.02   7.765    199
       3098.26   7.753    190
       3096.06   7.747    545
       3093.68   7.741     81
       2857.58   7.151    140
       2854.83   7.144    213
       2850.44   7.133   1000
       2849.34   7.130    923
       2846.96   7.124    359
       2845.86   7.121    277
       2843.11   7.115    195
       2840.55   7.108    103
       2838.90   7.104    146
       1604.36   4.015     57
       1599.41   4.003     69
       1594.46   3.990    107
       1590.25   3.980    107
       1585.31   3.967     75
       1580.54   3.955     62
       1210.55   3.030     95
       1205.78   3.018     99
       1196.81   2.995    126
       1192.05   2.983    115
       1102.66   2.760    123
       1092.77   2.735    128
       1088.92   2.725    110
       1079.03   2.700     99
    

in DMSO-d6



KBr disc



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