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网站主页CAS数据库列表 645-45-4更多图谱氢化肉桂酰氯(645-45-4)核磁图(13CNMR)

氢化肉桂酰氯

产品名称 氢化肉桂酰氯

CAS号645-45-4

分子式C9H9ClO

分子量168.62

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  • Mass

    MS-NW-7791          
    3-phenylpropionyl chloride
    C9H9ClO             (Mass of molecular ion:    168)
    

       Source Temperature: 240 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          26.0       1.5
          27.0       8.1
          36.0       2.4
          37.0       1.2
          38.0       3.0
          39.0      12.6
          41.0       1.4
          42.0       1.5
          49.0       1.1
          50.0      10.8
          51.0      23.9
          51.5       1.1
          52.0       5.5
          52.5       1.2
          53.0       1.8
          55.0       2.6
          61.0       1.2
          62.0       3.4
          63.0       8.1
          64.0       1.8
          65.0      12.5
          66.0       1.1
          66.5       1.8
          74.0       3.7
          75.0       2.9
          76.0       3.3
          77.0      24.9
          78.0      18.7
          79.0      12.5
          89.0       4.3
          90.0       1.7
          91.0     100.0
          92.0       8.1
         102.0       3.3
         103.0      22.3
         104.0      86.5
         105.0      89.1
         106.0       7.6
         125.0       1.4
         131.0       8.7
         132.0      12.4
         133.0      17.3
         134.0       1.7
         168.0      26.2
         169.0       2.9
         170.0       9.0
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C9 H9 Cl O 0.05 ml : 0.5 ml CDCl3
    3-phenylpropionyl chloride
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.38 to 7.08 B 3.10 C 2.97

         Hz     ppm     Int.
    

        663.25   7.406     39
        662.19   7.394     36
        661.44   7.386     30
        659.44   7.364     72
        657.44   7.341     67
        655.75   7.322    125
        655.31   7.317    116
        653.88   7.302    143
        651.31   7.273    305
        649.44   7.252    533
        647.38   7.229   1000
        646.56   7.220    876
        644.19   7.193    978
        640.63   7.154    339
        635.75   7.099    174
        632.94   7.068     98
        627.63   7.008     32
        627.13   7.003     31
        626.81   6.999     31
        291.75   3.258    114
        290.19   3.241     36
        288.19   3.218    188
        286.69   3.202    137
        284.75   3.180     78
        281.75   3.146    611
        280.94   3.137    451
        277.88   3.103    177
        276.63   3.089    594
        275.50   3.077    680
        270.63   3.022    524
        269.81   3.013    475
        264.63   2.955    424
        262.25   2.929     94
        259.56   2.899    133
        258.13   2.883    134
        254.56   2.843     93
    

in CDCl3



liquid film