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网站主页CAS数据库列表 64415-07-2更多图谱7-三氟甲基-4-硫醇喹啉(64415-07-2)红外图谱(IR1)

7-三氟甲基-4-硫醇喹啉

产品名称 7-三氟甲基-4-硫醇喹啉

CAS号64415-07-2

分子式C10H6F3NS

分子量229.22


  • Mass

    MS-IW-0567          
    7-trifluoromethyl-4-quinolinethiol
    C10H6F3NS           (Mass of molecular ion:    229)
    

       Source Temperature: 180 °C
       Sample Temperature: 110 °C
       Direct, 75 eV
    

          18.0       1.4
          45.0       1.7
          58.0       3.0
          63.0       1.1
          69.0       3.3
          74.0       1.3
          75.0       2.0
          76.0       1.7
          81.0       1.0
          87.0       1.1
          93.0       1.1
          97.5       1.0
          99.0       1.5
         107.0       1.4
         114.5       3.8
         119.0       1.3
         132.0       1.8
         137.0       2.2
         138.0       1.2
         145.0       6.1
         149.0       1.1
         157.0       5.2
         158.0       1.2
         159.0       2.0
         160.0       1.7
         165.0       2.4
         166.0       1.1
         169.0       7.5
         172.0      22.4
         173.0       2.0
         176.0       2.2
         181.0       1.7
         184.0       1.8
         185.0      13.2
         186.0       1.3
         188.0       1.2
         190.0       1.4
         196.0       5.0
         197.0       1.0
         201.0       6.5
         202.0       1.7
         208.0       3.3
         209.0       7.8
         210.0       4.0
         228.0      10.0
         229.0     100.0
         230.0      13.4
         231.0       5.2
    

400 MHz in DMSO-d6


  • 1H NMR 399.65 MHz
    C10 H6 F3 N S 0.036 g : 0.5 ml DMSO-d6
    7-trifluoromethyl-4-quinolinethiol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 13.158 B 8.855 C 8.05 D 8.014 E 7.751 F 7.427 J(B,E)=8.8HZ J(D,F)=6.6HZ

         Hz     ppm     Int.
    

       5258.79  13.159    168
       3543.46   8.867    437
       3534.67   8.845    456
       3218.99   8.055    643
       3218.26   8.053    626
       3206.30   8.023    498
       3199.71   8.007    521
       3102.78   7.764    347
       3101.32   7.761    363
       3094.24   7.743    340
       3092.77   7.739    354
       3092.29   7.738    353
       2971.44   7.436   1000
       2964.84   7.419    924
    

in DMSO-d6



KBr disc



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