图谱信息 供应商 相关产品
网站主页CAS数据库列表 643-28-7更多图谱2-异丙基苯胺(643-28-7)ESR图谱

2-异丙基苯胺

产品名称 2-异丙基苯胺

CAS号643-28-7

分子式C9H13N

分子量135.21

展开


  • Mass

    MS-NW-2220          
    o-isopropylaniline
    C9H13N              (Mass of molecular ion:    135)
    

       Source Temperature: 270 °C
       Sample Temperature: 170 °C
       Reservoir, 75 eV
    

          27.0       1.8
          28.0       1.3
          39.0       4.4
          41.0       2.4
          42.0       1.9
          50.0       1.0
          51.0       3.0
          52.0       1.7
          53.0       1.3
          54.0       1.0
          58.5       1.9
          60.0       1.9
          63.0       1.7
          65.0       4.7
          66.0       1.8
          77.0       8.9
          78.0       2.0
          79.0       1.3
          89.0       1.0
          91.0       5.9
          92.0       1.9
          93.0       6.3
          94.0       4.3
         102.0       1.1
         103.0       7.2
         104.0       1.3
         106.0       6.0
         115.0       1.4
         117.0       2.6
         118.0       4.8
         119.0       4.0
         120.0     100.0
         121.0       9.5
         134.0       1.7
         135.0      35.9
         136.0       3.6
         162.0       4.0
         177.0       1.5
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C9 H13 N 0.04 ml : 0.5 ml CDCl3
    o-isopropylaniline
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.13 B 7.02 C 6.75 D 6.66 E 3.6 F 2.87 G 1.248

         Hz     ppm     Int.
    

        643.38   7.184     92
        642.13   7.170     38
        641.63   7.165     53
        636.19   7.104     79
        634.38   7.084    104
        628.94   7.023     89
        627.06   7.002     68
        621.56   6.941     91
        619.69   6.920     63
        613.63   6.852     54
        613.19   6.847     55
        611.94   6.833     74
        611.56   6.829     70
        606.25   6.770     50
        605.81   6.765     58
        604.63   6.752     69
        604.25   6.747     71
        599.44   6.694    100
        598.94   6.688    113
        597.81   6.675     80
        597.38   6.671     79
        591.94   6.610     52
        591.44   6.604     57
        590.38   6.593     48
        589.94   6.588     46
        317.19   3.542     53
        264.94   2.959     33
        258.13   2.883     45
        251.31   2.807     38
        114.94   1.284   1000
        112.88   1.261     73
        110.38   1.233     33
        109.50   1.223     64
        108.19   1.209    866
    

in CDCl3



CCl4 solution



liquid film





OXIDATION WITH PERBENZOIC ACID