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MassMS-NW-9482 3-morpholino-1,2-propanediol C7H15NO3 (Mass of molecular ion: 161)
Source Temperature: 260 °C Sample Temperature: 150 °C Reservoir, 75 eV
15.0 1.5 27.0 1.6 28.0 4.4 29.0 3.2 30.0 2.5 31.0 1.6 41.0 2.1 42.0 9.6 43.0 4.4 44.0 2.1 45.0 1.4 55.0 1.1 56.0 15.6 57.0 3.2 58.0 1.9 70.0 4.1 72.0 1.9 86.0 1.1 87.0 1.2 100.0 100.0 101.0 6.0 102.0 1.0 130.0 8.8 161.0 1.7
400 MHz in CDCl3
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1H NMR 399.65 MHz C7 H15 N O3 0.05 ml : 0.5 ml CDCl3 3-morpholino-1,2-propanediol 
Assign. Shift(ppm)
A 3.97 B 3.840 C 3.72 D *1 3.677 E *1 3.506 F *2 2.62 G *3 2.516 J *2 2.46 K *3 2.369
Hz ppm Int.1587.28 3.972 357 1546.02 3.869 86 1542.11 3.859 170 1540.77 3.856 131 1537.96 3.849 157 1536.74 3.846 255 1532.96 3.836 262 1531.62 3.833 158 1528.93 3.826 141 1527.59 3.823 188 1523.68 3.813 105 1491.33 3.732 600 1489.50 3.728 627 1487.67 3.723 708 1485.72 3.718 1000 1483.89 3.713 675 1481.93 3.709 653 1480.22 3.704 597 1477.42 3.697 485 1473.63 3.688 400 1468.63 3.675 92 1465.94 3.669 505 1462.16 3.659 456 1409.06 3.526 468 1403.69 3.513 444 1397.58 3.498 368 1392.21 3.484 341 1058.96 2.650 150 1054.08 2.638 208 1047.73 2.622 251 1042.72 2.610 319 1038.33 2.599 197 1017.70 2.547 300 1008.54 2.524 293 1005.13 2.516 426 995.97 2.493 440 992.19 2.483 192 987.92 2.472 288 982.54 2.459 227 976.68 2.444 207 971.92 2.432 143 952.64 2.384 443 948.49 2.374 458 940.06 2.353 332 935.91 2.342 320
in CDCl3
liquid film
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