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MS-IW-2169 1-(p-fluorophenyl)piperazine dihydrochloride C10H13FN2 2HCl (Mass of molecular ion: 180)
Source Temperature: 150 °C Sample Temperature: 150 °C Direct, 75 eV
18.0 1.0 28.0 3.2 29.0 2.9 30.0 1.9 35.0 1.7 36.0 17.9 38.0 6.0 42.0 1.7 56.0 6.7 57.0 4.1 75.0 2.8 90.0 1.5 95.0 7.9 96.0 1.4 109.0 4.1 122.0 10.0 123.0 11.1 124.0 4.5 125.0 1.0 138.0 100.0 139.0 9.2 150.0 1.1 180.0 35.8 181.0 4.2
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C10 H13 F N2 0.032 g : 0.5 ml DMSO-d6 1-(p-fluorophenyl)piperazine dihydrochloride Assign. Shift(ppm)
A 9.78 B 7.170 C 6.56 D 3.451 E 3.273
Hz ppm Int.
3908.54 9.780 70 2868.96 7.179 1000 2862.40 7.163 963 2620.24 6.557 194 1384.74 3.465 215 1379.85 3.453 311 1374.36 3.439 282 1308.29 3.274 232
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