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网站主页CAS数据库列表 638-29-9更多图谱正戊酰氯(638-29-9)质谱(MS)

正戊酰氯

产品名称 正戊酰氯

CAS号638-29-9

分子式C5H9ClO

分子量120.58

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  • Mass

    MS-NW-5338          
    valeryl chloride
    C5H9ClO             (Mass of molecular ion:    120)
    

       Source Temperature: 270 °C
       Sample Temperature: 190 °C
       Reservoir, 75 eV
    

          14.0       1.5
          15.0       4.0
          26.0      10.9
          27.0      61.0
          28.0      28.5
          29.0      80.1
          30.0       2.1
          31.0       1.0
          35.0       1.7
          36.0       7.8
          37.0       2.4
          38.0       4.6
          39.0      30.5
          40.0       4.3
          41.0      80.2
          42.0      29.6
          43.0      25.1
          45.0       3.2
          49.0       1.9
          50.0       3.4
          51.0       3.1
          52.0       1.0
          53.0       3.5
          54.0       1.4
          55.0      43.9
          56.0      18.0
          57.0      93.8
          58.0       4.5
          60.0      34.1
          61.0       1.9
          63.0       5.8
          65.0       2.0
          73.0      14.0
          74.0       1.8
          77.0       1.1
          78.0      34.0
          79.0       2.9
          80.0      11.3
          81.0       1.0
          83.0       1.2
          84.0      12.2
          85.0     100.0
          86.0       6.0
          87.0       1.4
          91.0      10.5
          92.0       4.4
          93.0       3.7
          94.0       1.6
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C5 H9 Cl O 0.04 ml : 0.5 ml CDCl3
    valeryl chloride
    ChemicalStructure
        Assign.     Shift(ppm)
    A 2.879 B 1.67 C 1.40 D 0.93

         Hz     ppm     Int.
    

        265.94   2.970    309
        258.75   2.890    717
        255.13   2.849     62
        254.81   2.846     60
        254.50   2.842     62
        251.63   2.810    515
        168.13   1.878     48
        166.94   1.865     52
        160.69   1.795    162
        158.81   1.774     88
        158.13   1.766    112
        156.38   1.747     72
        153.81   1.718    256
        152.50   1.703    215
        151.63   1.694    161
        150.88   1.685    173
        149.00   1.664     87
        146.19   1.633    234
        145.44   1.624    239
        143.69   1.605    115
        142.81   1.595     97
        141.75   1.583    135
        140.00   1.564    137
        139.25   1.555    168
        138.31   1.545    117
        136.38   1.523    133
        135.19   1.510    160
        134.56   1.503    200
        132.81   1.483     72
        132.19   1.476     77
        130.19   1.454    181
        129.31   1.444    192
        128.44   1.435    193
        127.00   1.419    242
        125.38   1.400    108
        124.75   1.393    102
        124.38   1.389    102
        122.88   1.373    205
        120.38   1.345    255
        118.19   1.320    108
        116.63   1.303    102
        113.81   1.271    221
        112.56   1.257    127
        107.25   1.198     98
         91.25   1.019    324
         90.19   1.008    551
         89.63   1.001    487
         87.00   0.972     99
         86.06   0.961    107
         83.75   0.936   1000
         77.50   0.866    210
         76.31   0.853    273
         74.50   0.832    167
         71.50   0.799     45
         70.94   0.793     41
         69.81   0.780     36
    

in CDCl3



liquid film