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网站主页CAS数据库列表 637-53-6更多图谱硫代乙酰苯胺(637-53-6)红外图谱(IR3)

硫代乙酰苯胺

产品名称 硫代乙酰苯胺

CAS号637-53-6

分子式C8H9NS

分子量151.23

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  • Mass

    MS-NW-4859          
    thioacetanilide
    C8H9NS              (Mass of molecular ion:    151)
    

       Source Temperature: 270 °C
       Sample Temperature: 180 °C
       Reservoir, 75 eV
    

          15.0       1.7
          26.0       2.0
          27.0       4.2
          28.0       3.0
          32.0       1.7
          33.0       1.2
          34.0       1.3
          37.0       3.6
          38.0       7.2
          39.0      19.2
          40.0       3.8
          41.0       3.7
          42.0      19.9
          43.0       2.6
          45.0       3.9
          49.0       1.7
          50.0      15.7
          51.0      39.7
          52.0       6.6
          53.0       1.0
          54.0       1.4
          57.0       2.0
          58.0       8.1
          59.0      69.4
          60.0       3.0
          61.0       4.9
          62.0       3.7
          63.0       8.7
          64.0       4.8
          65.0      20.1
          66.0      16.9
          67.0       2.3
          69.0       2.7
          73.0       1.5
          74.0       5.9
          74.5       1.5
          75.0       4.6
          75.5       1.3
          76.0       4.9
          77.0      78.8
          78.0       9.3
          83.0       1.1
          84.0       1.4
          89.0       2.4
          90.0       2.4
          91.0       7.3
          92.0       6.5
          93.0     100.0
          94.0       7.3
         103.0       1.2
         104.0       2.6
         106.0       1.1
         108.0       2.3
         109.0      18.6
         110.0      41.2
         111.0       4.0
         112.0       2.1
         116.0       1.5
         117.0      25.9
         118.0      43.6
         119.0       4.4
         124.0       1.2
         135.0       3.3
         136.0       5.2
         149.0       1.7
         150.0      67.4
         151.0      89.0
         152.0      11.4
         153.0       4.4
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C8 H9 N S 0.035 g : 0.5 ml CDCl3
    thioacetanilide
    ChemicalStructure
        Assign.     Shift(ppm)
    A *1 10.0 B *1 9.2 C *2 7.633 D *3 7.42 E *3 7.37 F *4 7.34 G *4 7.249 J *2 7.150 K *5 2.683 L *5 2.493 ABUNDANT FORM UNCERTAIN.

         Hz     ppm     Int.
    

       3056.34   7.648    132
       3054.96   7.645    169
       3053.13   7.640     54
       3048.71   7.629    105
       3047.64   7.626    174
       3046.57   7.624    160
       2973.48   7.441     38
       2972.41   7.438     55
       2965.24   7.420    140
       2963.71   7.416     80
       2958.98   7.404     52
       2957.46   7.401    107
       2954.86   7.394     33
       2954.10   7.392     35
       2952.12   7.387    103
       2950.29   7.383     48
       2944.79   7.369    188
       2943.42   7.365    119
       2941.28   7.360     82
       2940.06   7.357     55
       2938.23   7.353     66
       2936.55   7.348    139
       2934.11   7.342     85
       2904.21   7.267     50
       2903.14   7.265     79
       2901.92   7.262     49
       2897.34   7.250     42
       2895.66   7.246    103
       2893.98   7.242     34
       2888.18   7.227     43
       2862.09   7.162    106
       2860.72   7.159    149
       2858.58   7.153     40
       2854.77   7.144     62
       2853.55   7.141    108
       2852.94   7.139     98
       2852.48   7.138     98
       1072.54   2.684   1000
        996.40   2.494    813
    

in CDCl3



CCl4 solution



KBr disc



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