2-氨基-4-氯-5-硝基苯酚

产品名称 2-氨基-4-氯-5-硝基苯酚

CAS号6358-07-2

分子式C6H5ClN2O3

分子量188.57

¹HNMR

¹³CNMR

IR1

IR2

Mass

MS-NW-8273          
2-amino-4-chloro-5-nitrophenol
C6H5ClN2O3          (Mass of molecular ion:    188)

   Source Temperature: 160 °C
   Sample Temperature: 120 °C
   Direct, 75 eV

      17.0       1.4
      18.0       5.1
      27.0       2.0
      28.0      18.1
      29.0       2.5
      30.0       6.2
      36.0       2.0
      37.0       2.9
      38.0       3.4
      38.5       2.1
      39.0       4.8
      40.0       2.2
      41.0       4.5
      42.0       2.2
      44.0       2.1
      46.0       1.2
      49.0       4.2
      50.0      15.1
      51.0      30.9
      52.0      20.2
      53.0       9.5
      54.0       5.4
      55.0       1.1
      57.0       2.3
      60.0       1.3
      61.0       5.1
      62.0      14.4
      63.0       7.4
      64.0       3.1
      65.0       3.1
      66.0       5.7
      67.0       4.1
      68.0       2.1
      69.0       1.1
      72.0       2.1
      73.0       5.9
      74.0       1.4
      75.0       6.0
      76.0      12.5
      77.0       6.6
      78.0      52.0
      79.0       8.9
      80.0       1.7
      85.0       2.7
      86.0       2.8
      87.0      47.5
      88.0       5.1
      89.0      16.6
      90.0       3.4
      94.0       1.8
      95.0       1.0
      97.0      20.4
      98.0       1.7
      99.0       6.9
     100.0       1.0
     101.0       1.3
     102.0       2.0
     106.0       1.5
     107.0       4.1
     112.0       2.1
     113.0       9.9
     114.0      43.6
     115.0       6.8
     116.0      14.3
     117.0       1.2
     124.0       1.9
     125.0       5.4
     126.0       1.0
     127.0       1.8
     129.0       1.5
     130.0      25.8
     131.0       2.1
     132.0       8.2
     141.0       4.3
     142.0      36.9
     143.0       4.6
     144.0      12.0
     145.0       1.0
     158.0      82.8
     159.0       5.9
     160.0      27.2
     161.0       1.9
     172.0       3.5
     174.0       1.1
     187.0       1.3
     188.0     100.0
     189.0       9.5
     190.0      33.2
     191.0       2.9

400 MHz in DMSO-d6

¹H NMR	399.65 MHz
C₆ H₅ Cl N₂ O₃	0.036 g : 0.5 ml CDCl₃
2-amino-4-chloro-5-nitrophenol

    Assign.     Shift(ppm)

      A            10.4
      B             7.526
      C             6.723
      D             6.33

     Hz     ppm     Int.

   4134.52  10.346     28
   3008.12   7.527    813
   2686.92   6.724   1000
   2530.98   6.333    378

in DMSO-d6

KBr disc

nujol mull

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