1-氨基-9-芴酮

Mass

MS-NW-6327          
1-amino-9-fluorenone
C13H9NO             (Mass of molecular ion:    195)

   Source Temperature: 240 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      18.0       4.3
      27.0       1.1
      31.0       2.4
      39.0       3.0
      44.0       1.3
      45.0       1.7
      50.0       1.3
      51.0       1.9
      52.0       1.1
      62.0       1.7
      63.0       2.8
      65.0       2.3
      66.0      10.5
      69.0       1.1
      69.5       3.4
      70.0       1.9
      70.5       3.0
      74.0       1.4
      75.0       1.6
      76.0       1.1
      77.0       1.4
      82.5       1.8
      83.5       6.3
      84.0       1.7
      87.0       1.5
      88.0       1.1
      89.0       1.7
      91.0       1.5
      97.5       3.6
      98.0       2.2
     113.0       1.7
     114.0       1.8
     115.0       1.9
     132.0       6.8
     133.0       5.1
     138.0       1.4
     139.0      14.0
     140.0       6.6
     141.0       1.1
     164.0       1.6
     166.0       5.0
     167.0       4.8
     168.0      12.8
     169.0       1.9
     194.0       1.3
     195.0     100.0
     196.0      15.0
     197.0       1.3

Assign. Shift(ppm) A 7.596 B 7.451 C 7.407 D 7.251 E 7.180 F 6.802 G 6.472 J 5.53

     Hz     ppm     Int.

   3039.79   7.607    715
   3036.25   7.598     85
   3032.35   7.588    793
   2983.03   7.465    468
   2975.71   7.446    994
   2967.41   7.426    509
   2966.31   7.423    520
   2963.50   7.416     79
   2960.08   7.407    744
   2958.98   7.404    744
   2955.08   7.395     68
   2952.64   7.389    329
   2951.54   7.386    327
   2905.52   7.271    442
   2904.42   7.268    454
   2898.19   7.252    780
   2897.09   7.250    765
   2890.87   7.234    340
   2889.77   7.231    345
   2886.60   7.223     38
   2877.56   7.201    531
   2870.36   7.183    686
   2869.26   7.180    694
   2865.60   7.171     65
   2862.06   7.162    620
   2858.15   7.152     32
   2721.68   6.811   1000
   2718.75   6.803     92
   2714.60   6.793    917
   2590.58   6.483    948
   2586.91   6.473     67
   2582.15   6.462    899
   2209.47   5.529    492