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2,3,4,5-四氯苯胺

产品名称 2,3,4,5-四氯苯胺

CAS号634-83-3

分子式C6H3Cl4N

分子量230.91

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  • Mass

    MS-NW-6812          
    2,3,4,5-tetrachloroaniline
    C6H3Cl4N            (Mass of molecular ion:    229)
    

       Source Temperature: 270 °C
       Sample Temperature: 190 °C
       Reservoir, 75 eV
    

          18.0       2.9
          28.0       1.2
          35.0       1.1
          36.0       2.0
          37.0       1.4
          44.0       1.2
          47.0       1.2
          49.0       1.0
          52.0       1.5
          60.0       1.8
          61.0       6.2
          61.5       3.3
          62.0       4.5
          62.5       1.2
          71.0       1.5
          72.0       1.8
          73.0       1.9
          75.0       1.6
          79.5       4.5
          80.5       2.7
          83.0       2.0
          84.0       1.1
          85.0       1.3
          86.0       2.5
          87.0       1.3
          88.0       2.3
          89.0       4.4
          95.0       1.5
          96.0       4.8
          96.5       2.6
          97.0       4.2
          97.5       2.4
          98.0       3.2
          98.5       1.0
          99.0       2.3
         107.0       2.9
         108.0       1.4
         109.0       1.9
         114.5       4.4
         115.5       5.9
         116.5       2.8
         122.0       3.6
         123.0       2.1
         124.0       5.2
         125.0       1.0
         126.0       1.4
         131.0       6.0
         132.0       1.1
         133.0       4.6
         135.0       1.2
         157.0       1.5
         158.0      14.9
         159.0       7.0
         160.0      10.5
         161.0       4.2
         162.0       2.0
         167.0      10.9
         168.0       1.3
         169.0      10.0
         171.0       3.6
         193.0       4.5
         194.0       6.7
         195.0       5.4
         196.0       6.6
         197.0       2.7
         198.0       2.2
         201.0       2.4
         203.0       3.0
         205.0       1.5
         229.0      78.4
         230.0       6.4
         231.0     100.0
         232.0       7.5
         233.0      47.7
         234.0       3.6
         235.0      10.6
         237.0       1.0
    

400 MHz in CDCl3

parameter in CDCl3


  • 1H NMR 399.65 MHz
    C6 H3 Cl4 N 0.040 g : 0.5 ml CDCl3
    2,3,4,5-tetrachloroaniline
    ChemicalStructure
        Assign.     Shift(ppm)
    A 6.804 B 4.25

         Hz     ppm     Int.
    

       2719.48   6.805   1000
       1699.22   4.252    130
    


  • 1H NMR 300 MHz
    C6 H3 Cl4 N 0.048 g : 0.5 ml CDCl3
    2,3,4,5-tetrachloroaniline
    ChemicalStructure
        Parameter     ppm  Hz
    D(A) 6.803 D(B) 4.20

         Hz     ppm     Int.
    

       2040.89   6.803   1000
       1259.99   4.200     90
    

in CDCl3



KBr disc



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