1-氨基吡咯烷盐酸盐

产品名称 1-氨基吡咯烷盐酸盐

CAS号63234-71-9

分子式C4H11ClN2

分子量122.6

¹³CNMR

Mass

MS-NW-6300          
N-aminopyrrolidine hydrochloride
C4H10N2 HCl         (Mass of molecular ion:     86)

   Source Temperature: 260 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      25.0       1.5
      26.0      14.9
      27.0      42.9
      28.0      52.9
      29.0      34.0
      30.0      28.3
      31.0       3.0
      32.0       2.0
      35.0       6.0
      36.0      46.3
      37.0       2.0
      38.0      14.1
      39.0      22.7
      40.0       6.4
      41.0      48.8
      42.0      82.2
      43.0      37.2
      44.0      31.3
      45.0       7.2
      50.0       2.3
      51.0       3.5
      52.0       2.6
      53.0       4.5
      54.0       9.7
      55.0      23.8
      56.0      26.5
      57.0      18.1
      58.0      40.2
      59.0       1.5
      64.0       2.0
      66.0       2.5
      67.0       3.1
      68.0      16.8
      69.0      13.9
      70.0       4.3
      71.0       2.0
      80.0       1.3
      81.0       2.2
      82.0       2.5
      83.0      35.1
      84.0      81.5
      85.0     100.0
      86.0      87.6
      87.0       5.0

90 MHz in CDCl3

400 MHz in DMSO-d6

¹H NMR	89.56 MHz
C₄ H₁₀ N₂	0.042 g : 0.5 ml CDCl₃
N-aminopyrrolidine hydrochloride

    Assign.     Shift(ppm)

      A             7.5
      B             3.57
      C             2.13

     Hz     ppm     Int.

    675.94   7.548    376
    327.06   3.652    291
    320.00   3.574    816
    313.06   3.496    368
    198.13   2.213    352
    194.25   2.169    414
    191.00   2.133   1000
    187.44   2.093    407
    187.13   2.090    407
    183.88   2.054    296

¹H NMR	399.65 MHz
C₄ H₁₀ N₂	0.040 g : 0.5 ml DMSO-d₆
N-aminopyrrolidine hydrochloride

    Assign.     Shift(ppm)

      A             3.19
      B             1.90

     Hz     ppm     Int.

   1274.54   3.190    359
    760.25   1.903   1000

in DMSO-d6

in CDCl3

KBr disc

nujol mull

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1-氨基吡咯烷盐酸盐(63234-71-9)核磁图(¹³CNMR) 相关产品图谱

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