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戊酸烯丙酯

产品名称 戊酸烯丙酯

CAS号6321-45-5

分子式C8H14O2

分子量142.2

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  • Mass

    MS-NW-5725          
    allyl valerate
    C8H14O2             (Mass of molecular ion:    142)
    

       Source Temperature: 260 °C
       Sample Temperature: 190 °C
       Reservoir, 75 eV
    

          15.0       1.9
          26.0       2.3
          27.0      14.5
          28.0       5.9
          29.0      35.2
          30.0       1.3
          31.0       2.1
          38.0       1.3
          39.0      18.0
          40.0       3.1
          41.0      72.2
          42.0       4.1
          43.0       8.3
          44.0       1.1
          45.0       1.6
          54.0       4.1
          55.0      18.4
          56.0       6.1
          57.0      92.2
          58.0       6.2
          59.0       5.5
          60.0       4.8
          73.0       2.7
          82.0       1.9
          83.0       5.4
          84.0       1.5
          85.0     100.0
          86.0       6.0
          99.0       1.3
         100.0      15.5
         101.0       2.3
         103.0       2.4
         113.0       2.7
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C8 H14 O2 0.04 ml : 0.5 ml CDCl3
    allyl valerate
    ChemicalStructure
        Assign.     Shift(ppm)
    A 5.91 B 5.32 C 5.23 D 4.576 E 2.34 F 1.62 G 1.36 J 0.93 J(A,B)=17.3HZ. J(A,C)=10.0HZ. J(A,D)=5.5HZ.

         Hz     ppm     Int.
    

        551.23   6.155     57
        545.59   6.092    106
        541.15   6.043     77
        540.12   6.031     64
        535.60   5.981    131
        534.06   5.964     99
        530.21   5.921     78
        528.33   5.900    176
        523.97   5.851    128
        522.95   5.840    115
        518.33   5.788    232
        512.95   5.728    151
        485.44   5.421    101
        484.07   5.405    244
        483.73   5.402    247
        482.19   5.384    363
        480.82   5.369    169
        474.58   5.300    148
        473.47   5.287    295
        472.28   5.274    215
        471.68   5.267    212
        470.48   5.254    110
        468.35   5.230     82
        466.81   5.213    176
        465.01   5.193    208
        463.39   5.175    241
        461.60   5.155    194
        460.40   5.141    100
        413.75   4.620    373
        412.46   4.606    625
        411.18   4.592    363
        408.19   4.558    336
        406.99   4.545    587
        405.63   4.530    327
        217.47   2.429    199
        216.53   2.418    204
        213.45   2.384     50
        209.95   2.345    513
        206.27   2.304     57
        205.93   2.300     55
        202.43   2.261    405
        161.41   1.803     52
        160.39   1.791     71
        153.98   1.720    190
        151.42   1.691    150
        149.28   1.667     79
        147.14   1.643    204
        145.86   1.629    212
        145.52   1.625    212
        144.07   1.609    161
        139.03   1.553    273
        135.69   1.516    143
        131.85   1.473    236
        128.60   1.436     77
        125.18   1.398    196
        123.82   1.383    189
        121.77   1.360     89
        119.46   1.334    169
        117.07   1.308    214
        113.56   1.268     81
        110.66   1.236    187
        104.08   1.163     89
         88.61   0.990    552
         84.85   0.948     66
         82.29   0.919   1000
         76.14   0.851    176
         74.77   0.835    220
         72.97   0.815    111
    

in CDCl3



liquid film



4880 A,200 M,liquid