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MassMS-IW-0865 tris(2-methylallyl)amine C12H21N (Mass of molecular ion: 179)
Source Temperature: 210 °C Sample Temperature: 150 °C Reservoir, 75 eV
27.0 2.3 29.0 7.1 30.0 2.2 39.0 3.5 41.0 4.0 42.0 4.4 43.0 1.9 44.0 1.2 53.0 2.1 55.0 32.2 56.0 3.6 58.0 1.0 67.0 6.8 68.0 2.0 69.0 2.0 70.0 2.3 80.0 1.3 81.0 3.1 82.0 8.0 83.0 1.1 84.0 4.1 94.0 1.5 95.0 1.6 96.0 2.7 108.0 3.2 109.0 2.8 110.0 1.2 111.0 1.0 122.0 2.6 123.0 5.6 124.0 2.5 136.0 7.7 137.0 1.0 138.0 100.0 139.0 10.3 164.0 12.4 165.0 1.6 178.0 1.3 179.0 12.2 180.0 1.8
400 MHz in CDCl3
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1H NMR 399.65 MHz C12 H21 N 0.05 ml : 0.5 ml CDCl3 tris(2-methylallyl)amine 
Assign. Shift(ppm)
A *1 4.899 B *1 4.822 C 2.784 D 1.734
Hz ppm Int.1958.74 4.902 220 1957.52 4.899 247 1956.54 4.896 227 1929.08 4.827 177 1927.61 4.824 235 1926.76 4.822 239 1925.29 4.818 193 1112.55 2.784 696 693.36 1.735 866 692.38 1.733 1000
in CDCl3
liquid film
