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MassMS-NW-2923 thiopropionamide C3H7NS (Mass of molecular ion: 89)
Source Temperature: 280 °C Sample Temperature: 180 °C Reservoir, 75 eV
15.0 2.6 18.0 1.8 26.0 5.4 27.0 10.2 28.0 37.9 29.0 7.1 30.0 7.4 32.0 3.3 33.0 3.1 34.0 6.4 39.0 2.0 40.0 1.5 41.0 1.9 42.0 4.2 44.0 2.6 45.0 6.4 46.0 1.0 47.0 1.2 51.0 2.2 52.0 3.7 53.0 1.6 54.0 17.8 55.0 3.4 56.0 28.1 57.0 1.7 58.0 1.5 59.0 4.4 60.0 68.7 61.0 8.6 62.0 3.3 71.0 7.6 72.0 10.3 73.0 2.7 74.0 1.4 87.0 1.7 88.0 5.2 89.0 100.0 90.0 4.8 91.0 4.6
90 MHz in CDCl3
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1H NMR 89.56 MHz C3 H7 N S 0.055 g : 0.5 ml CDCl3 thiopropionamide 
Assign. Shift(ppm)
A 7.6 B 2.695 C 1.304
Hz ppm Int.672.75 7.512 52 253.25 2.828 125 252.63 2.821 126 250.38 2.796 25 249.81 2.790 28 245.25 2.739 441 242.56 2.709 38 237.75 2.655 495 235.00 2.624 35 233.63 2.609 29 232.75 2.599 30 230.75 2.577 171 230.19 2.571 173 123.75 1.382 553 121.13 1.353 58 120.25 1.343 57 116.38 1.300 1000 108.81 1.215 421
in CDCl3
KBr disc
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