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MassMS-IW-6145 2,3-dimethoxyaniline C8H11NO2 (Mass of molecular ion: 153)
Source Temperature: 200 °C Sample Temperature: 150 °C Reservoir, 75 eV
15.0 1.1 28.0 3.2 33.5 1.1 38.0 1.5 39.0 5.8 40.0 1.2 41.0 5.6 50.0 1.2 51.0 2.8 52.0 4.7 53.0 3.3 54.0 1.0 63.0 1.1 65.0 7.5 66.0 3.1 67.0 9.9 68.0 1.1 76.5 1.1 77.0 1.5 78.0 1.9 79.0 2.3 80.0 5.3 81.0 1.0 82.0 1.5 90.0 3.0 92.0 10.9 93.0 10.9 94.0 2.7 95.0 26.9 96.0 2.1 106.0 1.2 107.0 1.2 108.0 11.0 109.0 3.3 110.0 12.7 111.0 1.2 120.0 2.0 137.0 2.2 138.0 100.0 139.0 8.3 153.0 81.3 154.0 7.9
400 MHz in CDCl3
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1H NMR 399.65 MHz C8 H11 N O2 0.05 ml : 0.5 ml CDCl3 2,3-dimethoxyaniline 
Assign. Shift(ppm)
A 6.819 B 6.353 C 6.313 D *1 3.806 E *1 3.799 F 3.8
Hz ppm Int.2734.01 6.842 138 2725.83 6.821 261 2717.65 6.801 162 2543.70 6.365 158 2542.36 6.362 184 2535.64 6.345 153 2534.30 6.342 167 2527.83 6.326 143 2526.49 6.322 122 2519.65 6.305 130 2518.19 6.301 115 1521.12 3.807 939 1518.43 3.800 1000
in CDCl3
liquid film
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