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2-氯-5-羟基三氟甲苯

产品名称 2-氯-5-羟基三氟甲苯

CAS号6294-93-5

分子式C7H4ClF3O

分子量196.55

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  • Mass

    MS-KW-0171          
    4-chloro-3-(trifluoromethyl)phenol
    C7H4ClF3O           (Mass of molecular ion:    196)
    

       Source Temperature: 250 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          18.0       1.9
          28.0       1.9
          31.0       1.1
          37.0       1.4
          38.0       1.8
          39.0       1.9
          50.0       1.4
          53.0       2.1
          57.0       2.0
          61.0       2.1
          62.0       3.6
          63.0       9.2
          64.0       1.1
          66.0       3.1
          69.0       2.2
          73.0       3.2
          74.0       2.2
          75.0       3.2
          80.0       2.8
          80.5       1.1
          81.0       1.8
          83.0       3.7
          88.0       1.2
          91.0       1.2
          93.0       1.0
          97.0       1.1
          98.0       1.9
          99.0       5.5
         101.0       1.5
         113.0       8.0
         114.0       2.2
         117.0       1.2
         131.0       1.1
         132.0       7.2
         133.0       4.5
         141.0       2.3
         146.0       7.7
         147.0       1.6
         148.0      12.6
         149.0       1.6
         150.0       3.4
         161.0      19.8
         162.0       2.0
         167.0       1.8
         175.0       1.5
         177.0      14.4
         178.0       1.3
         179.0       6.0
         195.0       1.8
         196.0     100.0
         197.0       8.4
         198.0      32.5
         199.0       2.5
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C7 H4 Cl F3 O 0.043 g : 0.5 ml CDCl3
    4-chloro-3-(trifluoromethyl)phenol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.347 B 7.164 C 6.938 D 5.38

         Hz     ppm     Int.
    

       2940.67   7.359    350
       2940.06   7.357    355
       2931.76   7.336    384
       2931.40   7.335    389
       2864.50   7.168    504
       2861.57   7.161    515
       2778.69   6.953    265
       2778.08   6.952    257
       2775.63   6.946    241
       2775.15   6.944    235
       2770.02   6.932    237
       2769.41   6.930    231
       2766.97   6.924    216
       2766.48   6.923    207
       2151.00   5.383   1000
    

in CDCl3



KBr disk



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