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MassMS-IW-1885 (o-nitrophenyl)hydrazine monohydrochloride C6H7N3O2 HCl (Mass of molecular ion: 153)
Source Temperature: 130 °C Sample Temperature: 120 °C Direct, 75 eV
18.0 1.4 27.0 3.2 28.0 6.5 29.0 3.0 30.0 4.3 31.0 1.0 35.0 5.6 36.0 48.1 37.0 3.8 38.0 17.0 39.0 12.8 40.0 1.9 41.0 1.9 43.0 1.0 50.0 13.4 51.0 35.7 52.0 96.3 53.0 20.7 54.0 2.5 61.0 1.9 62.0 4.2 63.0 17.0 64.0 15.5 65.0 10.0 66.0 1.8 74.0 4.1 75.0 3.8 76.0 10.4 76.5 2.9 77.0 100.0 78.0 29.7 79.0 25.0 80.0 7.3 90.0 14.9 91.0 22.4 92.0 6.7 93.0 2.2 105.0 5.4 106.0 1.6 107.0 1.8 119.0 5.0 135.0 9.6 136.0 2.4 153.0 84.2 154.0 6.6
400 MHz in DMSO-d6
90 MHz in D2O
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1H NMR 399.65 MHz C6 H7 N3 O2 saturated in DMSO-d6 (o-nitrophenyl)hydrazine monohydrochloride 
Assign. Shift(ppm)
A 10.6 B 9.25 C 8.164 D 7.760 E 7.392 F 7.104
Hz ppm Int.4234.44 10.596 51 3698.31 9.254 266 3268.06 8.178 941 3266.59 8.174 997 3259.63 8.157 987 3257.98 8.153 983 3110.35 7.783 444 3108.70 7.779 471 3104.86 7.769 131 3103.02 7.765 551 3101.74 7.762 881 3100.28 7.758 603 3094.60 7.744 542 3093.13 7.740 518 2958.87 7.404 878 2957.77 7.401 942 2950.26 7.383 819 2949.35 7.380 820 2847.51 7.126 544 2846.22 7.122 592 2840.18 7.107 616 2839.08 7.104 1000 2837.80 7.101 645 2831.75 7.086 526 2830.66 7.083 535
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1H NMR 89.56 MHz C6 H7 N3 O2 0.038 g : 0.5 ml D2O (o-nitrophenyl)hydrazine monohydrochloride Assign. Shift(ppm)
A 8.243 B 7.790 C 7.23 D 7.18 THE SOLVENT SIGNAL REMOVED.
Hz ppm Int.744.25 8.311 270 743.31 8.300 258 742.50 8.291 436 736.31 8.222 247 735.44 8.212 349 733.88 8.195 539 707.31 7.898 226 705.75 7.881 237 700.75 7.825 127 700.00 7.816 232 698.56 7.800 400 697.19 7.785 340 691.63 7.723 413 690.00 7.705 389 651.75 7.278 951 651.13 7.271 942 648.69 7.244 100 643.31 7.184 1000 642.00 7.169 482 636.06 7.103 273 634.81 7.089 225
in D2O
in DMSO-d6
KBr disc
liquid film
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