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MassMS-NW-9974 2,5-dichloropentylamine hydrochloride C5H11Cl2N HCl (Mass of molecular ion: 155)
Source Temperature: 160 °C Sample Temperature: 110 °C Direct, 75 eV
18.0 3.2 27.0 3.1 28.0 4.8 29.0 1.4 30.0 100.0 31.0 2.5 35.0 1.5 36.0 18.3 38.0 6.0 39.0 2.3 41.0 2.9 42.0 1.9 43.0 1.5 53.0 1.1 56.0 2.4 120.0 5.2 122.0 1.6
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C5 H11 Cl2 N 0.041 g : 0.5 ml DMSO-d6 2,5-dichloropentylamine hydrochloride 
Assign. Shift(ppm)
A 8.6 B 4.408 C 3.690 D *1 3.26 E *1 3.06 F 1.98 G 1.83
Hz ppm Int.3429.11 8.581 509 1770.94 4.432 144 1766.36 4.420 226 1762.39 4.410 278 1758.12 4.400 216 1753.85 4.389 161 1479.95 3.704 452 1478.88 3.701 490 1474.00 3.689 1000 1467.90 3.673 521 1308.90 3.276 136 1296.39 3.244 176 1226.81 3.070 128 1220.55 3.055 157 1211.55 3.032 96 808.72 2.024 175 807.19 2.020 237 803.22 2.010 173 799.26 2.000 200 795.29 1.990 264 793.30 1.985 191 789.64 1.976 187 788.42 1.973 186 785.06 1.965 171 781.86 1.957 179 778.96 1.950 213 775.45 1.941 206 740.97 1.855 215 739.29 1.850 236 735.47 1.841 257 731.81 1.832 310 729.98 1.827 324 726.47 1.818 271 723.72 1.811 320 722.35 1.808 311
in D2O
in DMSO-d6
KBr disc
nujol mull
