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网站主页CAS数据库列表 629-98-1更多图谱13-二十二烯醇(629-98-1)核磁图(13CNMR)

13-二十二烯醇

产品名称 13-二十二烯醇

CAS号629-98-1

分子式C22H44O

分子量324.58

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  • Mass

    MS-IW-4083          
    cis-13-docosen-1-ol
    C22H44O             (Mass of molecular ion:    324)
    

       Source Temperature: 150 °C
       Sample Temperature: 110 °C
       Direct, 75 eV
    

          18.0       3.0
          27.0       3.6
          28.0       1.3
          29.0      12.2
          31.0       6.3
          39.0       4.0
          41.0      44.4
          42.0       8.4
          43.0      40.6
          44.0       1.7
          53.0       3.8
          54.0      24.0
          55.0      82.9
          56.0      20.2
          57.0      33.1
          58.0       1.6
          65.0       1.1
          66.0       6.2
          67.0      43.8
          68.0      41.5
          69.0      59.1
          70.0      16.6
          71.0      13.8
          72.0       1.1
          77.0       1.0
          79.0       4.3
          80.0       6.0
          81.0      48.2
          82.0     100.0
          83.0      58.9
          84.0      10.3
          85.0       8.5
          86.0       1.0
          93.0       1.6
          94.0       3.4
          95.0      44.6
          96.0      93.7
          97.0      43.8
          98.0       7.0
          99.0       2.3
         108.0       1.5
         109.0      27.9
         110.0      36.0
         111.0      17.3
         112.0       3.9
         113.0       1.2
         122.0       2.4
         123.0      20.3
         124.0      26.4
         125.0       8.1
         126.0       2.4
         136.0       1.6
         137.0      14.2
         138.0      18.3
         139.0       4.4
         140.0       1.6
         151.0       5.6
         152.0      10.4
         153.0       2.6
         154.0       1.1
         165.0       3.2
         166.0       7.0
         167.0       1.8
         179.0       2.2
         180.0       5.2
         181.0       1.2
         193.0       1.7
         194.0       4.4
         195.0       1.0
         207.0       1.4
         208.0       3.8
         221.0       1.1
         222.0       3.5
         235.0       1.0
         236.0       3.4
         249.0       1.6
         250.0       4.2
         263.0       1.2
         264.0       3.0
         278.0       4.4
         306.0      29.9
         307.0       7.3
         324.0       1.2
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C22 H44 O 0.031 g : 0.5 ml CDCl3
    cis-13-docosen-1-ol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 5.35 B 3.635 C 2.013 D 1.561 E 1.31 F 1.27 G 0.880

         Hz     ppm     Int.
    

       2142.46   5.361     88
       2137.82   5.350    179
       2136.84   5.347     93
       2133.30   5.338     90
       1459.72   3.653    104
       1453.00   3.636    210
       1446.41   3.620    109
        814.21   2.038     54
        807.74   2.022    146
        802.00   2.007    137
        795.29   1.990     69
        632.57   1.583     50
        625.37   1.565     72
        625.00   1.564     72
        617.92   1.547     69
        530.15   1.327    185
        529.79   1.326    185
        524.90   1.314    228
        505.98   1.267   1000
        359.01   0.899    109
        352.29   0.882    358
        345.34   0.865    137
    

in CDCl3



KBr disc



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