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MS-NW-2814 tetradecane C14H30 (Mass of molecular ion: 198)
Source Temperature: 260 °C Sample Temperature: 180 °C Reservoir, 75 eV
27.0 6.9 28.0 1.2 29.0 16.4 39.0 4.2 41.0 26.2 42.0 8.7 43.0 74.1 44.0 2.5 53.0 1.3 54.0 1.4 55.0 14.4 56.0 14.4 57.0 100.0 58.0 4.8 67.0 1.1 68.0 1.1 69.0 6.8 70.0 11.8 71.0 64.4 72.0 3.3 83.0 3.7 84.0 7.5 85.0 42.4 86.0 2.7 97.0 2.4 98.0 5.5 99.0 8.0 112.0 3.6 113.0 5.2 126.0 2.5 127.0 4.3 140.0 1.6 141.0 3.6 155.0 2.5 169.0 1.5 198.0 5.1
400 MHz in CDCl3
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1H NMR 399.65 MHz C14 H30 0.05 ml : 0.5 ml CDCl3 tetradecane Assign. Shift(ppm)
A 1.26 B 0.880
Hz ppm Int.
530.88 1.329 53 527.95 1.322 64 518.19 1.297 149 504.88 1.264 1000 502.44 1.258 884 492.55 1.233 174 479.98 1.202 35 365.11 0.914 28 358.89 0.899 172 354.74 0.888 123 352.17 0.882 477 349.85 0.876 192 345.09 0.864 230
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