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网站主页CAS数据库列表 629-04-9更多图谱1-溴代庚烷(629-04-9)质谱(MS)

1-溴代庚烷

产品名称 1-溴代庚烷

CAS号629-04-9

分子式C7H15Br

分子量179.1

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  • Mass

    MS2015-05121CW      
    1-bromoheptane
    C7H15Br             (Mass of molecular ion:    178)
    

       Source Temperature: 250 °C
       Sample Temperature: 250 °C
       Reservoir, 70 eV
    

          14.0       1.1
          18.0       1.5
          26.0       1.7
          27.0      10.2
          29.0      14.8
          38.0       1.3
          39.0       9.2
          40.0       5.0
          41.0      43.9
          42.0      13.9
          43.0      37.5
          44.0       2.6
          50.0       1.1
          51.0       2.2
          52.0       1.0
          53.0       7.2
          54.0       5.6
          55.0      43.5
          56.0      34.0
          57.0      92.9
          58.0       8.2
          65.0       1.1
          67.0       4.0
          68.0       3.0
          69.0      29.0
          70.0      13.4
          71.0       5.1
          81.0       1.4
          83.0       3.9
          84.0       1.1
          85.0       3.9
          93.0       1.4
          95.0       1.4
          97.0       1.6
          98.0      16.8
          99.0       2.4
         107.0       6.1
         109.0       5.8
         121.0       1.1
         135.0      64.2
         136.0       4.6
         137.0     100.0
         138.0       4.3
         149.0       6.4
         151.0       6.3
         178.0       2.2
         180.0       2.3
    

in CDCl3

90 MHz in CDCl3




  • 1H NMR 89.56 MHz
    C7 H15 Br 0.04 ml : 0.5 ml CDCl3
    1-bromoheptane
    ChemicalStructure
        Assign.     Shift(ppm)
    A 0.89 B 1.14 to 1.61 C 1.847 D 3.399

         Hz     ppm     Int.
    

        311.63   3.480    384
        309.88   3.461     41
        304.81   3.404   1000
        297.94   3.327    542
        296.31   3.309     39
        173.19   1.934    101
        166.50   1.860    158
        159.56   1.782    138
        118.06   1.319    855
         84.88   0.948    191
         79.50   0.888    724
         73.38   0.820    143
    

in CDCl3



CCl4 solution



liquid film



4880 A,200 M,liquid