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网站主页CAS数据库列表 6286-43-7更多图谱1,2,3-环已三醇(6286-43-7)质谱(MS)

1,2,3-环已三醇

产品名称 1,2,3-环已三醇

CAS号6286-43-7

分子式C6H12O3

分子量132.16

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  • Mass

    MS-NW-9384          
    1,2,3-cyclohexanetriol
    C6H12O3             (Mass of molecular ion:    132)
    

       Source Temperature: 140 °C
       Sample Temperature: 110 °C
       Direct, 75 eV
    

          15.0       1.3
          18.0       1.5
          19.0       1.4
          27.0       5.6
          28.0       2.7
          29.0      10.6
          30.0       1.5
          31.0       5.4
          39.0       4.7
          40.0       1.7
          41.0       9.9
          42.0       6.8
          43.0       8.6
          44.0       7.9
          45.0       2.8
          47.0       1.6
          53.0       1.5
          55.0       8.1
          56.0       1.4
          57.0      40.4
          58.0      17.3
          59.0       1.1
          60.0       7.3
          67.0       5.3
          68.0       5.8
          69.0       6.2
          70.0     100.0
          71.0       8.2
          73.0       7.1
          79.0       1.1
          81.0       2.0
          83.0       7.5
          86.0       8.3
          95.0       2.1
          96.0       9.3
          97.0       3.7
         113.0       4.4
         114.0      17.3
         115.0       2.9
    

400 MHz in D2O


  • 1H NMR 399.65 MHz
    C6 H12 O3 0.044 g : 0.5 ml D2O
    1,2,3-cyclohexanetriol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 4.055 B 3.785 C 3.441 D 1.901 E 1.758 F 1.55 G 1.318 ASSIGNED BY C-H COSY

         Hz     ppm     Int.
    

       1625.24   4.067    243
       1622.56   4.060    440
       1619.75   4.053    518
       1617.55   4.048    390
       1607.30   4.022     34
       1606.93   4.021     32
       1514.16   3.789    227
       1509.64   3.778    241
       1505.25   3.767    312
       1504.15   3.764    335
       1500.73   3.756    338
       1499.63   3.753    323
       1495.24   3.742    293
       1490.72   3.731    280
       1380.86   3.456    520
       1377.81   3.448    504
       1372.19   3.434    460
       1369.02   3.426    459
        771.24   1.930    163
        768.92   1.924    193
        767.33   1.921    240
        765.01   1.915    163
        762.82   1.909    200
        760.99   1.905    138
        758.30   1.898    224
        756.23   1.893    210
        754.15   1.888    259
        751.95   1.882    176
        749.76   1.877    123
        713.75   1.786    101
        708.86   1.774    226
        706.91   1.769    185
        705.20   1.765    194
        703.61   1.761    243
        700.44   1.753    168
        697.88   1.747    265
        693.60   1.736    178
        636.96   1.594    107
        635.50   1.591     99
        633.54   1.586    114
        631.96   1.582    105
        627.56   1.571    198
        623.29   1.560    660
        621.70   1.556    734
        620.48   1.553    718
        617.68   1.546   1000
        613.77   1.536    881
        605.59   1.516    241
        601.20   1.505    119
        598.51   1.498    104
        545.04   1.364     97
        538.82   1.349    137
        534.91   1.339    150
        532.23   1.332    183
        528.81   1.324    225
        525.63   1.316    169
        522.22   1.307    196
        519.17   1.300    159
        516.60   1.293    186
        506.35   1.267     89
    

in D2O



KBr disc



nujol mull