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2-氯-5-硝基苯胺

产品名称 2-氯-5-硝基苯胺

CAS号6283-25-6

分子式C6H5ClN2O2

分子量172.57

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  • Mass

    MS-NW-1374          
    2-chloro-5-nitroaniline
    C6H5ClN2O2          (Mass of molecular ion:    172)
    

       Source Temperature: 260 °C
       Sample Temperature: 180 °C
       Reservoir, 75 eV
    

          18.0       1.8
          27.0       1.2
          28.0       4.0
          30.0       3.5
          37.0       4.1
          38.0       7.0
          39.0      11.1
          40.0       2.2
          41.0       5.5
          42.0       1.0
          44.0       1.1
          44.5       1.5
          49.0       1.8
          50.0       2.7
          51.0       5.4
          52.0      17.7
          53.0       2.3
          54.0       1.1
          61.0       5.3
          62.0      10.5
          63.0      36.7
          64.0      10.1
          65.0       7.4
          66.0       5.8
          73.0      10.1
          74.0       2.8
          75.0       4.8
          76.0       1.5
          78.0       4.3
          79.0       1.7
          86.0       1.2
          87.0       2.3
          88.0       1.7
          89.0       3.5
          90.0     100.0
          91.0      15.3
          97.0       1.1
          98.0       1.0
          99.0      31.2
         100.0       3.3
         101.0      10.0
         102.0       1.1
         106.0       2.3
         114.0      20.6
         115.0       1.5
         116.0       6.7
         125.0       3.5
         126.0      67.6
         127.0       6.1
         128.0      22.1
         129.0       1.6
         142.0       7.2
         144.0       2.8
         156.0       1.0
         172.0      96.5
         173.0       7.4
         174.0      31.6
         175.0       2.3
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C6 H5 Cl N2 O2 0.05 g : 0.5 ml CDCl3
    2-chloro-5-nitroaniline
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.61 B 7.52 C 7.38 D 4.3

         Hz     ppm     Int.
    

        685.44   7.654     48
        683.56   7.633    332
        682.81   7.625    463
        681.13   7.606    888
        680.38   7.597    964
        677.81   7.569     84
        677.50   7.565     89
        676.19   7.551     43
        674.13   7.528     45
        671.50   7.498    954
        669.13   7.472    711
        666.88   7.447     71
        666.44   7.442     74
        666.00   7.437     60
        665.44   7.431     58
        663.38   7.408   1000
        662.63   7.399    845
        654.94   7.313    294
        654.25   7.306    287
        384.38   4.292    114
    

in CDCl3



KBr disc



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