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MS-NW-7288 1,5-diiodopentane C5H10I2 (Mass of molecular ion: 324)
Source Temperature: 220 °C Sample Temperature: 190 °C Reservoir, 75 eV
26.0 1.1 27.0 16.2 29.0 4.9 38.0 1.6 39.0 16.9 40.0 3.3 41.0 74.8 42.0 9.9 43.0 7.1 53.0 3.0 55.0 5.4 67.0 2.5 69.0 86.4 70.0 6.8 127.0 8.4 128.0 4.7 141.0 4.8 154.0 1.3 155.0 54.7 156.0 1.3 169.0 9.3 197.0 100.0 198.0 5.7 211.0 1.1 254.0 2.2 324.0 8.8
90 MHz in CDCl3
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1H NMR 89.56 MHz C5 H10 I2 0.05 ml : 0.5 ml CDCl3 1,5-diiodopentane Assign. Shift(ppm)
A 3.194 B 1.85 C 1.54
Hz ppm Int.
292.88 3.271 374 286.19 3.196 1000 279.50 3.121 564 181.50 2.027 70 180.56 2.017 73 173.69 1.940 246 171.88 1.920 152 167.06 1.866 405 163.38 1.825 153 160.38 1.791 355 153.56 1.715 168 150.50 1.681 89 149.38 1.668 97 148.81 1.662 100 146.94 1.641 135 143.88 1.607 140 140.63 1.571 192 139.25 1.555 126 135.75 1.516 131 135.44 1.513 131 134.50 1.502 131 133.19 1.488 132 130.38 1.456 85 129.19 1.443 69 127.19 1.421 56 126.75 1.416 57 125.19 1.398 68
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