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MS-KW-0249 2-methoxyethyl chloroformate C4H7ClO3 (Mass of molecular ion: 138)
Source Temperature: 240 °C Sample Temperature: 150 °C Reservoir, 75 eV
15.0 13.4 26.0 1.2 27.0 7.5 28.0 4.2 29.0 14.0 30.0 1.2 31.0 5.8 36.0 1.7 42.0 1.0 43.0 6.0 44.0 5.5 45.0 100.0 46.0 2.3 49.0 1.3 58.0 14.5 59.0 11.5 62.0 7.2 63.0 13.7 64.0 2.9 65.0 4.5 77.0 1.8 89.0 2.6
400 MHz in CDCl3
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1H NMR 399.65 MHz C4H7ClO3 0.05 ml : 0.5 ml CDCl3 2-methoxyethyl chloroformate Assign. Shift(ppm)
A 4.455 B 3.661 C 3.402
Hz ppm Int.
1785.53 4.467 310 1782.72 4.460 202 1781.01 4.455 260 1779.06 4.451 197 1776.37 4.444 308 1468.02 3.673 301 1465.21 3.666 187 1463.38 3.661 251 1461.55 3.656 181 1458.87 3.650 276 1359.75 3.402 1000
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