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MS-IW-9739 diethyl telluride C4H10Te (Mass of molecular ion: 188)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
12.0 1.1 14.0 4.5 25.0 2.3 26.0 20.0 27.0 67.8 28.0 31.9 29.0 100.0 30.0 2.8 31.0 3.5 35.0 8.5 36.0 37.8 37.0 13.3 38.0 12.3 39.0 4.5 41.0 5.9 43.0 10.9 44.0 1.6 45.0 1.6 47.0 9.5 49.0 10.0 51.0 2.1 122.0 4.5 123.0 3.3 124.0 10.4 125.0 17.1 126.0 40.7 127.0 21.1 128.0 62.8 129.0 29.0 130.0 74.7 131.0 31.4 132.0 20.7 139.0 2.1 140.0 2.1 141.0 3.5 142.0 2.6 143.0 4.7 144.0 2.6 145.0 3.5 151.0 2.6 152.0 4.5 153.0 6.1 154.0 11.6 155.0 24.5 156.0 22.6 157.0 26.4 158.0 36.6 159.0 26.4 160.0 38.8 171.0 1.1 173.0 1.4 180.0 4.7 181.0 1.9 182.0 9.2 183.0 13.5 184.0 34.7 185.0 1.6 186.0 57.3 187.0 2.6 188.0 61.1 189.0 2.8 250.0 1.6 251.0 1.6 252.0 3.0 253.0 2.3 254.0 5.4 255.0 1.9 256.0 8.0 258.0 7.3 260.0 3.8
parameter neat
400 MHz in CDCl3
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1H NMR 300 MHz C4 H10 Te neat diethyl telluride Parameter ppm Hz
D(A) 1.512 D(B) 2.467 J(A,B) 7.6 BREUNINGER,V. ET AL. BER.BUNSENGES.PHYS.CHEM. 70, 613 (1966)
Hz ppm Int.
751.65 2.505 143 744.02 2.480 459 736.42 2.455 483 728.86 2.430 169 461.10 1.537 509 453.51 1.512 1000 445.91 1.486 454
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1H NMR 399.65 MHz C4 H10 Te 30 mg : 0.5 ml CDCl3 di Assign. Shift(ppm)
A 2.653 B 1.630
Hz ppm Int.
1071.78 2.682 213 1064.09 2.663 525 1056.40 2.644 518 1048.83 2.625 182 664.55 1.663 129 662.96 1.659 147 658.81 1.649 579 656.74 1.644 123 651.12 1.630 1000 643.43 1.610 510
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