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MS-NW-1055 1,4-dibromopentane C5H10Br2 (Mass of molecular ion: 228)
Source Temperature: 240 °C Sample Temperature: 170 °C Reservoir, 75 eV
18.0 1.4 26.0 1.8 27.0 16.8 29.0 6.2 38.0 1.5 39.0 12.8 40.0 2.4 41.0 62.1 42.0 8.1 43.0 11.8 53.0 4.0 55.0 5.1 67.0 2.4 68.0 1.1 69.0 100.0 70.0 5.8 107.0 6.4 109.0 6.0 121.0 1.0 149.0 30.9 150.0 2.5 151.0 29.3 152.0 1.7
90 MHz in CDCl3
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1H NMR 89.56 MHz C5 H10 Br2 0.02 ml : 0.5 ml CDCl3 1,4-dibromopentane Assign. Shift(ppm)
A 4.15 B 3.44 C 2.22 to 1.72 D 1.739
Hz ppm Int.
314.88 3.516 69 314.50 3.512 77 310.38 3.466 80 309.69 3.458 107 308.44 3.444 264 303.13 3.385 88 302.38 3.377 109 183.88 2.054 82 182.25 2.035 138 181.00 2.021 153 179.44 2.004 154 178.56 1.994 138 178.06 1.989 156 177.25 1.980 167 176.44 1.971 173 175.31 1.958 117 174.38 1.948 88 173.25 1.935 77 171.44 1.915 78 170.88 1.908 104 159.00 1.776 1000 152.31 1.701 931
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