3-[(p-nitrophenyl)hydrazono]butan-2-one oxime
产品名称 3-[(p-nitrophenyl)hydrazono]butan-2-one oxime
CAS号62454-83-5
分子式C10H12N4O3
分子量236.23
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MassMS-NW-6908 biacetyl mono(p-nitrophenylhydrazone) monooxime C10H12N4O3 (Mass of molecular ion: 236)
Source Temperature: 230 °C Sample Temperature: 170 °C Direct, 75 eV
15.0 15.4 17.0 2.4 18.0 9.7 26.0 1.8 27.0 7.9 28.0 9.5 29.0 1.6 30.0 74.7 31.0 4.9 37.0 1.6 38.0 6.4 39.0 13.3 40.0 6.4 41.0 14.9 42.0 44.8 43.0 8.4 44.0 3.0 50.0 8.1 51.0 6.6 52.0 11.2 53.0 7.7 54.0 4.0 55.0 2.5 57.0 1.4 58.0 11.6 61.0 1.0 62.0 5.0 63.0 26.1 64.0 25.7 65.0 9.9 66.0 1.9 67.0 1.4 68.0 8.0 69.0 6.8 70.0 4.7 74.0 2.3 75.0 8.3 76.0 10.7 77.0 4.3 78.0 4.6 79.0 10.3 80.0 9.2 81.0 3.6 82.0 1.0 83.0 4.1 84.0 3.2 88.0 1.0 89.0 5.2 90.0 31.5 91.0 22.4 92.0 10.5 93.0 2.1 98.0 1.1 99.0 2.1 100.0 1.4 102.0 1.3 103.0 1.8 104.0 2.8 105.0 6.7 106.0 17.2 107.0 4.8 108.0 8.9 109.0 1.0 116.0 1.0 117.0 1.9 118.0 1.5 119.0 1.3 120.0 3.2 121.0 1.7 122.0 23.1 123.0 2.2 130.0 1.2 131.0 5.6 132.0 6.7 133.0 1.5 135.0 1.0 136.0 25.1 137.0 8.9 138.0 15.6 139.0 3.1 143.0 1.1 144.0 1.5 145.0 1.7 146.0 1.1 147.0 3.0 150.0 9.8 151.0 14.5 152.0 3.2 156.0 1.5 157.0 1.0 158.0 1.2 161.0 2.7 162.0 1.3 163.0 1.2 172.0 4.3 173.0 25.2 174.0 3.6 177.0 8.4 178.0 2.7 188.0 12.9 189.0 3.2 190.0 1.4 202.0 5.3 203.0 2.4 204.0 2.3 206.0 1.3 218.0 17.6 219.0 77.3 220.0 14.6 221.0 2.2 234.0 4.2 235.0 2.5 236.0 100.0 237.0 15.3 238.0 2.3
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C10 H12 N4 O3 0.036 g : 0.5 ml DMSO-d6 biacetyl mono(p-nitrophenylhydrazone) monooxime 
Assign. Shift(ppm)
A *1 11.4 B *1 10.2 C 8.143 D 7.324 E *2 2.153 F *2 2.082
Hz ppm Int.4577.14 11.453 184 4095.24 10.248 153 3259.45 8.156 272 3250.11 8.133 280 2934.69 7.344 34 2931.76 7.336 233 2927.18 7.325 22 2922.42 7.313 223 2919.49 7.306 31 860.52 2.154 940 832.13 2.083 1000
in DMSO-d6
KBr disc
nujol mull
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