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网站主页CAS数据库列表 623-37-0更多图谱3-己醇(623-37-0)核磁图(1HNMR)

3-己醇

产品名称 3-己醇

CAS号623-37-0

分子式C6H14O

分子量102.17

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  • Mass

    MS-NW-1157          
    3-hexanol
    C6H14O              (Mass of molecular ion:    102)
    

       Source Temperature: 240 °C
       Sample Temperature: 170 °C
       Reservoir, 75 eV
    

          15.0       1.3
          18.0       1.2
          19.0       1.0
          26.0       1.1
          27.0      12.6
          28.0       4.7
          29.0      11.4
          30.0       1.0
          31.0      37.4
          32.0       1.0
          39.0       6.3
          41.0      20.5
          42.0       3.1
          43.0      29.1
          44.0       3.4
          45.0       5.3
          53.0       1.2
          55.0      77.3
          56.0       5.5
          57.0       6.7
          58.0       8.0
          59.0     100.0
          60.0       3.6
          69.0       1.7
          72.0       4.4
          73.0      46.5
          74.0       2.2
          84.0       1.1
          85.0       1.9
         101.0       1.0
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C6 H14 O 0.04 ml : 0.5 ml CDCl3
    3-hexanol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 3.54 B 1.74 C 1.67 to 1.11 D 0.94

         Hz     ppm     Int.
    

        322.49   3.601     42
        321.46   3.590     51
        319.58   3.569     43
        316.25   3.532     72
        315.14   3.519     57
        313.26   3.498     42
        312.40   3.489     39
        311.89   3.483     40
        310.35   3.466     45
        309.84   3.460     45
        155.60   1.738    480
        147.66   1.649     45
        145.01   1.620     48
        142.36   1.590     46
        141.08   1.576     51
        139.28   1.556    135
        137.57   1.537    144
        136.04   1.519     72
        133.98   1.496    178
        131.34   1.467    379
        130.65   1.459    442
        129.46   1.446    311
        128.52   1.436    310
        126.72   1.415    335
        126.12   1.409    343
        125.18   1.398    310
        124.24   1.388    497
        120.74   1.349    158
        119.12   1.331    137
        117.75   1.315    126
        114.76   1.282     39
        113.90   1.272     43
        110.23   1.231     41
        109.03   1.218     32
        104.50   1.167     32
        103.82   1.160     31
         93.82   1.048     49
         91.69   1.024    271
         90.83   1.015    490
         90.06   1.006    383
         88.95   0.994    208
         84.08   0.939   1000
         83.40   0.932    739
         79.72   0.891    185
         78.36   0.875    155
         77.33   0.864    231
         76.31   0.853    260
         74.85   0.836    160
         73.57   0.822     69
         71.95   0.804     33
    

in CDCl3



CCl4 solution



liquid film



4880 A,200 M,liquid