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1-甲基-4-甲硫基苯

产品名称 1-甲基-4-甲硫基苯

CAS号623-13-2

分子式C8H10S

分子量138.23

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  • Mass

    MS-NW-7790          
    methyl p-tolyl sulfide
    C8H10S              (Mass of molecular ion:    138)
    

       Source Temperature: 240 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          15.0       1.6
          27.0       2.2
          38.0       1.7
          39.0      10.3
          41.0       1.5
          45.0      22.4
          46.0       1.2
          47.0       1.5
          50.0       3.1
          51.0       5.2
          52.0       1.6
          53.0       2.0
          61.0       1.0
          62.0       2.3
          63.0       6.1
          64.0       1.3
          65.0       7.6
          69.0       4.4
          70.0       1.3
          71.0       1.4
          77.0       8.8
          78.0       4.5
          79.0      11.6
          82.0       1.1
          89.0       3.5
          90.0       1.2
          91.0      53.7
          92.0      10.2
          93.0       1.6
          95.0       1.0
          97.0       1.9
         105.0       4.8
         108.0       1.8
         121.0       6.1
         122.0       4.1
         123.0      27.3
         124.0       2.6
         125.0       1.2
         137.0      11.7
         138.0     100.0
         139.0      10.4
         140.0       5.0
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C8 H10 S 0.05 ml : 0.5 ml CDCl3
    methyl p-tolyl sulfide
    ChemicalStructure
        Assign.     Shift(ppm)
    A *1 7.13 B *1 7.07 C 2.408 D 2.274

         Hz     ppm     Int.
    

        646.25   7.216     62
        643.69   7.188     44
        640.31   7.150     92
        637.63   7.120    425
        634.75   7.088    356
        628.75   7.021     57
        628.25   7.015     58
        626.19   6.992     71
        215.75   2.410   1000
        203.75   2.276    689
    

in CDCl3



liquid film