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MassMS-NW-6442 N-methyl-p-toluidine C8H11N (Mass of molecular ion: 121)
Source Temperature: 260 °C Sample Temperature: 190 °C Reservoir, 75 eV
27.0 1.9 28.0 1.5 30.0 1.2 38.0 1.0 39.0 4.9 41.0 1.5 42.0 1.2 50.0 2.2 51.0 4.8 52.0 3.4 53.0 2.1 58.5 2.4 59.5 5.6 60.0 1.9 60.5 3.4 62.0 1.3 63.0 3.5 64.0 1.2 65.0 7.5 66.0 1.2 77.0 8.6 78.0 4.3 79.0 5.0 80.0 1.4 89.0 2.5 90.0 1.8 91.0 17.4 92.0 4.7 93.0 2.5 104.0 2.5 105.0 1.6 106.0 8.3 107.0 1.5 118.0 4.0 119.0 4.3 120.0 100.0 121.0 94.1 122.0 8.1
90 MHz in CDCl3
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1H NMR 89.56 MHz C8 H11 N 0.05 ml : 0.5 ml CDCl3 N-methyl-p-toluidine 
Assign. Shift(ppm)
A 7.032 B 6.568 C 3.46 D 2.816 E 2.279
Hz ppm Int.634.31 7.083 183 626.19 6.992 254 591.44 6.604 293 583.00 6.510 192 309.81 3.460 262 252.25 2.817 1000 204.19 2.280 817
in CDCl3
liquid film
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