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网站主页CAS数据库列表 6228-47-3更多图谱三苯基丙基溴化膦(6228-47-3)核磁图(13CNMR)

三苯基丙基溴化膦

产品名称 三苯基丙基溴化膦

CAS号6228-47-3

分子式C21H22BrP

分子量385.28

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  • Mass

    MS-IW-6135          
    triphenylpropylphosphonium bromide
    C21H22BrP           (Mass of molecular ion:    384)
    

       Source Temperature: 180 °C
       Sample Temperature: 240 °C
       Direct, 75 eV
    

          27.0       2.5
          28.0       2.6
          39.0       4.0
          40.0       1.1
          41.0       6.5
          42.0       3.3
          43.0       7.0
          50.0       1.9
          51.0       3.7
          57.0       1.4
          65.0       1.0
          77.0       2.1
          78.0       2.4
          79.0       2.2
          80.0       6.5
          81.0       2.4
          82.0       6.4
          91.0       2.4
         107.0      12.6
         108.0      38.1
         109.0       4.1
         115.0       2.6
         122.0       1.3
         124.0       1.2
         131.0       2.3
         133.0       2.7
         139.0       1.4
         141.0       1.1
         152.0       6.8
         153.0       1.7
         154.0       1.7
         157.0       3.8
         170.0       2.0
         181.0       1.1
         183.0      63.4
         184.0      16.1
         185.0      10.6
         186.0       3.0
         199.0       1.9
         227.0       1.2
         228.0       2.1
         261.0      19.6
         262.0     100.0
         263.0      19.8
         264.0       1.9
         289.0      18.5
         290.0       4.1
         303.0       3.9
         304.0       4.0
         305.0       4.6
         306.0       1.0
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C21 H22 Br P 0.040 g : 0.5 ml CDCl3
    triphenylpropylphosphonium bromide
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.84 B 7.83 C 7.72 D 3.696 E 1.717 F 1.245

         Hz     ppm     Int.
    

       3145.39   7.871     88
       3143.55   7.866    459
       3142.33   7.863    655
       3140.75   7.859    326
       3137.45   7.851    229
       3135.25   7.845   1000
       3133.79   7.842    944
       3130.98   7.835    582
       3129.64   7.831    694
       3127.32   7.826    574
       3125.61   7.821    582
       3124.76   7.819    561
       3122.68   7.814    913
       3121.46   7.811    915
       3119.75   7.807    482
       3118.53   7.804    515
       3116.94   7.800    200
       3116.09   7.798    130
       3101.20   7.760    173
       3100.10   7.758    499
       3099.37   7.756    663
       3097.90   7.752    406
       3096.56   7.749    607
       3095.95   7.747    638
       3092.90   7.740    508
       3091.67   7.736    908
       3089.60   7.731    567
       3088.62   7.729    660
       3087.65   7.726    489
       3086.18   7.723    289
       3084.35   7.718    360
       3083.37   7.716    257
       3082.64   7.714    218
       3080.93   7.710    351
       3079.96   7.707    202
       3078.74   7.704     67
       1491.82   3.733    151
       1488.77   3.726     49
       1486.33   3.720     83
       1483.52   3.713    126
       1481.08   3.706    100
       1479.25   3.702    190
       1475.59   3.693    198
       1473.75   3.688    107
       1471.07   3.681    126
       1468.63   3.675     80
       1466.19   3.669     61
       1463.01   3.661    158
        703.25   1.760     69
        700.07   1.752     36
        697.63   1.746     54
        695.68   1.741    114
        694.46   1.738    131
        692.75   1.734     79
        690.55   1.728     78
        687.01   1.720    184
        683.72   1.711     81
        681.52   1.706     84
        679.57   1.701    137
        678.47   1.698    120
        676.39   1.693     58
        674.19   1.687     41
        670.90   1.679     76
        505.74   1.266    315
        503.91   1.261    326
        498.54   1.248    661
        496.70   1.243    674
        491.09   1.229    286
        489.38   1.225    280
    

in CDCl3



KBr disc



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