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网站主页CAS数据库列表 6222-17-9更多图谱1,6-二乙酰氧基己烷(6222-17-9)核磁图(1HNMR)

1,6-二乙酰氧基己烷

产品名称 1,6-二乙酰氧基己烷

CAS号6222-17-9

分子式C10H18O4

分子量202.25

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  • Mass

    MS-IW-6137          
    hexamethylene diacetate
    C10H18O4            (Mass of molecular ion:    202)
    

       Source Temperature: 210 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          15.0       3.1
          27.0       1.9
          28.0       2.6
          29.0       2.6
          31.0       1.1
          39.0       2.4
          41.0      11.2
          42.0       9.1
          43.0     100.0
          44.0       4.5
          45.0       1.0
          53.0       1.2
          54.0      57.9
          55.0      23.0
          56.0       2.4
          57.0       3.4
          58.0       3.2
          61.0      36.8
          67.0      50.5
          68.0       4.9
          69.0       3.9
          70.0       3.7
          71.0       8.9
          72.0       1.9
          73.0       9.8
          79.0       1.1
          80.0       1.6
          81.0      12.4
          82.0      87.0
          83.0      11.6
          84.0       8.5
          85.0       2.2
          86.0       2.3
          87.0       1.4
          94.0       1.2
          97.0       1.8
          98.0       1.2
          99.0      12.9
         100.0       4.3
         101.0       3.0
         103.0       2.0
         112.0       7.7
         114.0       1.9
         115.0       4.3
         203.0       1.4
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C10 H18 O4 0.05 ml : 0.5 ml CDCl3
    hexamethylene diacetate
    ChemicalStructure
        Assign.     Shift(ppm)
    A 4.062 B 2.049 C 1.640 D 1.394

         Hz     ppm     Int.
    

       1630.37   4.080    224
       1623.66   4.063    412
       1616.94   4.046    223
        818.85   2.049   1000
        670.65   1.679     23
        663.70   1.661     80
        661.13   1.655     65
        656.98   1.644    119
        652.34   1.633     67
        649.90   1.627     88
        644.04   1.612     30
        643.07   1.610     31
        563.84   1.411     94
        560.18   1.402    107
        558.96   1.399     99
        556.40   1.393    189
        552.98   1.384    101
        548.95   1.374     75
    

in CDCl3



liquid film