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MS-NW-7122 3-diethylamino-1,2-propanediol C7H17NO2 (Mass of molecular ion: 147)
Source Temperature: 280 °C Sample Temperature: 190 °C Reservoir, 75 eV
15.0 2.4 18.0 1.7 27.0 5.1 28.0 6.4 29.0 8.7 30.0 19.3 31.0 2.6 41.0 1.7 42.0 8.1 43.0 2.1 44.0 4.6 56.0 4.8 57.0 2.1 58.0 21.3 59.0 1.2 60.0 2.6 70.0 1.4 72.0 5.3 73.0 1.1 86.0 100.0 87.0 5.7 88.0 1.9 116.0 12.1 117.0 1.0 147.0 1.4
90 MHz in CDCl3
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1H NMR 89.56 MHz C7 H17 N O2 0.02 ml : 0.5 ml CDCl3 3-diethylamino-1,2-propanediol Assign. Shift(ppm)
A 3.69 B 3.45 C 2.53 D 1.038
Hz ppm Int.
339.44 3.791 81 330.75 3.694 164 329.25 3.677 109 327.25 3.654 103 321.50 3.590 116 309.19 3.453 153 236.31 2.639 218 233.81 2.611 234 229.06 2.558 292 227.00 2.535 274 222.13 2.481 243 220.06 2.458 213 99.69 1.114 525 92.69 1.035 1000 85.50 0.955 411
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