-
MassMS-NW-5417 m-phenetidine C8H11NO (Mass of molecular ion: 137)
Source Temperature: 260 °C Sample Temperature: 190 °C Reservoir, 75 eV
26.0 1.3 27.0 7.5 28.0 4.2 29.0 4.8 38.0 2.1 39.0 7.6 40.0 1.8 41.0 3.8 42.0 2.1 50.0 1.3 51.0 2.8 52.0 5.7 53.0 8.9 54.0 3.3 62.0 1.1 63.0 3.1 64.0 3.1 65.0 9.7 66.0 3.7 67.0 1.0 68.0 2.7 69.0 1.1 78.0 1.2 79.0 2.0 80.0 27.1 81.0 21.6 82.0 4.6 91.0 2.6 92.0 6.6 93.0 10.1 94.0 4.5 107.0 1.2 108.0 3.3 109.0 100.0 110.0 7.2 122.0 3.0 136.0 1.6 137.0 76.2 138.0 7.2 178.0 2.8 193.0 1.1
90 MHz in CDCl3
-
1H NMR 89.56 MHz C8 H11 N O 0.04 ml : 0.5 ml CDCl3 m-phenetidine 
Assign. Shift(ppm)
A 7.02 B 6.30 C 6.25 D 6.21 E 3.956 F 3.59 G 1.366 J(E,G)=6.99HZ.
Hz ppm Int.637.44 7.118 108 635.25 7.094 38 631.13 7.048 42 629.44 7.029 150 629.06 7.024 151 628.06 7.013 87 622.25 6.948 89 621.00 6.934 143 620.31 6.927 53 569.63 6.361 78 568.63 6.350 115 567.38 6.336 101 566.44 6.325 158 564.75 6.306 105 563.75 6.295 91 562.50 6.281 213 561.56 6.271 146 559.88 6.252 106 558.31 6.234 302 556.13 6.210 493 554.50 6.192 270 365.13 4.077 133 358.06 3.998 418 351.06 3.920 438 344.19 3.844 157 321.13 3.586 195 129.06 1.442 502 124.00 1.385 30 122.13 1.364 1000 115.13 1.286 439
in CDCl3
liquid film
更多供应商
