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MS-NW-9024 m-toluamide C8H9NO (Mass of molecular ion: 135)
Source Temperature: 260 °C Sample Temperature: 150 °C Reservoir, 75 eV
38.0 1.0 39.0 6.0 41.0 1.3 44.0 2.9 50.0 2.2 51.0 3.5 52.0 1.0 62.0 2.4 63.0 6.4 64.0 1.8 65.0 17.7 66.0 1.1 77.0 1.8 89.0 7.0 90.0 5.1 91.0 77.0 92.0 6.5 106.0 1.0 116.0 2.6 117.0 3.7 118.0 1.4 119.0 100.0 120.0 9.0 135.0 62.9 136.0 6.2
90 MHz in CDCl3
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1H NMR 89.56 MHz C8 H9 N O 0.036 g : 0.5 ml CDCl3 m-toluamide Assign. Shift(ppm)
A 7.66 B 7.65 C 7.35 D 7.34 E 6.6 F 2.357 CONFIRMED BY LAOCN PROGRAM
Hz ppm Int.
685.19 7.651 239 683.88 7.637 188 680.69 7.601 113 679.50 7.588 79 677.25 7.562 86 676.69 7.556 83 675.50 7.543 62 658.38 7.352 80 656.00 7.325 363 655.13 7.315 254 649.81 7.256 131 590.94 6.599 50 211.19 2.359 1000
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