3-氯苯甲酰氯

Mass

MS-NW-5124          
m-chlorobenzoyl chloride
C7H4Cl2O            (Mass of molecular ion:    174)

   Source Temperature: 260 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      28.0       1.3
      36.0       2.3
      37.0       3.7
      37.5       3.5
      38.0       7.5
      49.0       2.5
      50.0      16.2
      51.0       5.0
      55.5       4.4
      56.5       1.3
      61.0       1.8
      69.5       7.1
      70.5       2.4
      73.0       3.1
      74.0       9.3
      75.0      25.5
      76.0       6.5
      84.0       1.6
      85.0       3.3
      87.0       1.0
     110.0       1.1
     111.0      47.6
     112.0       3.5
     113.0      15.1
     114.0       1.1
     139.0     100.0
     140.0       7.9
     141.0      31.4
     142.0       2.6
     174.0      10.8
     175.0       1.1
     176.0       7.2
     178.0       1.2

Assign. Shift(ppm) A 8.05 B 8.00 C 7.633 D 7.471

     Hz     ppm     Int.

    726.50   8.112     36
    726.06   8.107     40
    723.69   8.081    229
    722.88   8.072    371
    721.94   8.061    731
    721.13   8.052   1000
    719.94   8.039    883
    719.56   8.035    881
    717.75   8.015    147
    716.50   8.001     89
    715.38   7.988     99
    713.75   7.970    438
    712.25   7.953    617
    710.56   7.934    342
    709.00   7.917     68
    706.88   7.893     30
    692.38   7.731     41
    691.06   7.717    180
    689.50   7.699    258
    687.50   7.677    212
    685.94   7.660     45
    683.00   7.627    533
    681.56   7.611    561
    681.06   7.605    578
    679.50   7.588    418
    675.06   7.538    577
    674.25   7.529    531
    671.88   7.503     62
    671.19   7.495     57
    670.81   7.491     54
    670.06   7.482     69
    667.69   7.456    432
    667.00   7.448    579
    666.19   7.439    234
    663.94   7.414     42
    662.56   7.398     37
    662.13   7.394     39
    659.81   7.368    172
    659.00   7.359    183