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MassMS-KW-0242 1-methyl-1-phenylhydrazine C7H10N2 (Mass of molecular ion: 122)
Source Temperature: 240 °C Sample Temperature: 150 °C Reservoir, 75 eV
15.0 1.8 16.0 1.0 17.0 1.1 18.0 1.9 27.0 3.3 28.0 5.1 29.0 9.6 30.0 2.2 37.0 1.4 38.0 3.2 39.0 9.8 40.0 1.0 41.0 1.0 42.0 1.1 43.0 4.9 45.0 1.8 50.0 8.2 51.0 23.9 52.0 7.3 52.5 1.1 53.0 4.1 53.5 1.7 61.0 3.9 62.0 1.4 63.0 5.2 64.0 3.7 65.0 8.3 66.0 2.8 74.0 2.7 75.0 2.0 76.0 2.2 77.0 90.2 78.0 17.3 79.0 21.9 80.0 2.5 90.0 1.0 91.0 4.3 92.0 6.9 93.0 7.6 94.0 2.0 104.0 11.6 105.0 10.7 106.0 25.0 107.0 68.5 108.0 5.4 121.0 8.6 122.0 100.0 123.0 8.7 133.0 3.4 134.0 3.9
400 MHz in CDCl3
90 MHz in CDCl3
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1H NMR 399.65 MHz C7H10N2 0.05 ml : 0.5 ml CDCl3 1-methyl-1-phenylhydrazine 
Assign. Shift(ppm)
A 7.208 B 6.924 C 6.765 D 3.56 E 2.983
Hz ppm Int.2892.09 7.235 40 2889.90 7.229 213 2888.92 7.227 99 2887.70 7.224 87 2884.89 7.217 53 2882.57 7.211 264 2881.72 7.209 180 2880.99 7.207 274 2878.79 7.201 55 2875.86 7.194 94 2874.52 7.191 102 2873.66 7.189 249 2871.46 7.183 44 2774.42 6.940 61 2772.34 6.935 264 2771.25 6.932 310 2770.39 6.930 180 2769.05 6.927 105 2765.51 6.918 93 2764.53 6.916 152 2763.43 6.913 260 2762.46 6.910 235 2760.01 6.904 42 2712.41 6.785 68 2711.31 6.782 116 2710.33 6.780 70 2705.08 6.767 112 2704.11 6.764 195 2703.01 6.762 111 2697.76 6.749 57 2696.78 6.746 99 2695.68 6.743 60 1421.03 3.555 153 1192.27 2.983 1000
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1H NMR 89.56 MHz C7 H10 N2 0.04 ml : 0.5 ml CDCl3 1-methyl-1-phenylhydrazine Assign. Shift(ppm)
A 7.23 B 6.98 C 6.80 D 3.59 E 3.061
Hz ppm Int.657.69 7.344 31 656.94 7.336 38 650.50 7.264 64 649.25 7.250 65 648.75 7.244 72 648.13 7.237 85 643.81 7.189 65 642.25 7.172 57 641.81 7.167 88 641.13 7.159 91 628.75 7.021 96 627.31 7.005 134 624.94 6.978 32 621.13 6.936 30 619.88 6.922 67 618.50 6.906 58 615.81 6.876 41 614.63 6.863 40 607.50 6.784 59 600.50 6.706 31 321.13 3.586 92 274.13 3.061 1000
in CDCl3
KBr disc
liquid film
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