400 MHz in D2O
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C6 H14 N2 O2 saturated in D2O DL-lysine dihydrochloride 
Assign. Shift(ppm)
A 4.104 B 3.028 C 1.99 D 1.738 E 1.53 SOLVENT PEAK REMOVED
Hz ppm Int.1646.48 4.120 536 1640.14 4.104 986 1636.60 4.096 106 1633.91 4.089 536 1223.88 3.063 41 1218.02 3.048 648 1210.33 3.029 990 1202.76 3.010 669 1198.12 2.998 44 833.98 2.087 89 828.13 2.073 164 823.24 2.060 137 822.39 2.058 150 819.46 2.051 259 817.38 2.046 235 815.92 2.042 106 813.72 2.037 437 811.40 2.031 184 808.84 2.024 345 807.98 2.022 328 802.86 2.009 689 799.80 2.002 99 798.95 2.000 113 796.63 1.994 560 793.82 1.987 106 791.99 1.982 283 789.92 1.977 324 788.21 1.973 181 786.25 1.968 338 785.52 1.966 341 781.62 1.956 171 779.66 1.951 304 777.71 1.946 150 777.47 1.946 150 775.51 1.941 116 771.85 1.932 137 771.00 1.930 143 765.14 1.915 113 710.69 1.779 246 702.88 1.759 775 695.07 1.740 1000 687.50 1.721 870 679.93 1.702 352 635.50 1.591 225 628.05 1.572 287 625.00 1.564 246 622.31 1.558 297 620.24 1.552 338 617.43 1.545 328 614.62 1.538 297 611.94 1.532 389 609.50 1.526 273 606.93 1.519 280 604.00 1.512 311 601.56 1.506 249 599.00 1.499 235 596.19 1.492 229
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1H NMR 399.65 MHz C6 H14 N2 O2 0.038 g : 0.5 ml DMSO-d6 DL-lysine dihydrochloride Assign. Shift(ppm)
A *1 8.59 B *1 8.25 C 3.844 D 2.766 E 1.839 F 1.621 G *2 1.501 J *2 1.406
Hz ppm Int.3433.53 8.592 996 3297.12 8.251 1000 1536.41 3.845 382 1098.02 2.748 589 746.15 1.868 307 738.53 1.848 746 731.66 1.831 788 724.18 1.813 390 663.15 1.660 154 655.82 1.641 466 648.35 1.623 675 640.87 1.604 561 633.54 1.586 260 617.37 1.545 158 610.05 1.527 218 603.64 1.511 293 596.31 1.493 306 588.84 1.474 179 572.66 1.433 201 565.19 1.415 281 558.32 1.398 258 551.61 1.381 205
in D2O
in DMSO-d6
KBr disc
nujol mull
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