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网站主页CAS数据库列表 616-14-8更多图谱1-碘-2-甲基丁烷(616-14-8)核磁图(1HNMR)

1-碘-2-甲基丁烷

产品名称 1-碘-2-甲基丁烷

CAS号616-14-8

分子式C5H11I

分子量198.05

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  • Mass

    MS-IW-9725          
    1-iodo-2-methylbutane
    C5H11I              (Mass of molecular ion:    198)
    

       Source Temperature: 230 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          27.0      11.4
          28.0       1.5
          29.0      22.4
          38.0       1.0
          39.0      11.1
          40.0       1.7
          41.0      35.2
          42.0       7.4
          43.0      99.7
          44.0       3.3
          53.0       2.1
          55.0      17.0
          56.0       1.4
          69.0       1.2
          70.0       1.9
          71.0     100.0
          72.0       5.6
         127.0       2.9
         128.0       3.6
         141.0       1.0
         169.0       2.5
         198.0      10.5
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C5 H11 I 0.05 ml : 0.5 ml CDCl3
    1-iodo-2-methylbutane
    ChemicalStructure
        Assign.     Shift(ppm)
    A *1 3.229 B *1 3.171 C 1.40 D 1.268 E 0.977 F 0.892

         Hz     ppm     Int.
    

       1299.32   3.252    160
       1294.68   3.240    149
       1289.67   3.227    314
       1285.03   3.216    279
       1273.56   3.187    270
       1267.70   3.173    284
       1263.92   3.163    133
       1258.18   3.149    139
        579.59   1.451     49
        573.85   1.436     96
        572.39   1.433     57
        568.60   1.423     63
        566.53   1.418    128
        565.06   1.414     68
        563.72   1.411     73
        562.26   1.407    127
        561.28   1.405    134
        559.33   1.400     89
        557.25   1.395    145
        556.40   1.393    163
        551.39   1.380    130
        550.17   1.377    132
        545.29   1.365     88
        539.31   1.350     39
        519.41   1.300     44
        518.55   1.298     55
        513.55   1.285     70
        512.21   1.282     88
        505.86   1.266    100
        504.88   1.264    106
        498.41   1.248     90
        393.80   0.986    957
        387.33   0.970    900
        368.65   0.923     45
        364.01   0.911    474
        356.69   0.893   1000
        352.17   0.882     67
        349.37   0.875    576
    

in CDCl3



liquid film