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MS-IW-3078 diallylamine hydrochloride C6H11N HCl (Mass of molecular ion: 97)
Source Temperature: 150 °C Sample Temperature: 110 °C Direct, 75 eV
15.0 2.8 17.0 1.4 18.0 5.9 26.0 3.6 27.0 11.0 28.0 45.5 29.0 5.7 30.0 18.5 35.0 9.7 36.0 68.1 37.0 3.7 38.0 23.4 39.0 47.1 40.0 6.1 41.0 99.2 42.0 21.3 43.0 13.3 44.0 1.3 52.0 2.5 53.0 2.2 54.0 16.7 55.0 9.9 56.0 32.7 57.0 2.3 65.0 1.3 67.0 8.3 68.0 88.3 69.0 12.8 70.0 100.0 71.0 5.6 77.0 1.5 79.0 3.5 80.0 7.8 81.0 6.8 82.0 66.8 83.0 4.0 94.0 5.1 96.0 35.0 97.0 40.8 98.0 3.0
90 MHz in CDCl3
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1H NMR 89.56 MHz C6 H11 N 0.047 g : 0.5 ml CDCl3 diallylamine hydrochloride Assign. Shift(ppm)
A 9.8 B 6.072 C 5.555 D 5.404 E 3.61
Hz ppm Int.
878.44 9.809 111 567.69 6.339 105 560.94 6.264 236 557.88 6.230 139 554.38 6.191 113 551.25 6.156 329 550.44 6.147 242 544.88 6.084 157 543.63 6.071 481 540.56 6.036 256 536.94 5.996 227 533.94 5.962 594 527.44 5.890 302 502.44 5.611 181 501.25 5.597 586 499.88 5.582 1000 498.81 5.570 443 495.25 5.530 872 494.44 5.521 629 493.88 5.515 539 486.63 5.434 287 485.56 5.422 623 484.06 5.405 557 483.38 5.398 484 482.56 5.389 609 481.50 5.377 271 325.75 3.638 479 325.44 3.634 482 325.06 3.630 481 322.63 3.603 461 321.38 3.589 469 320.75 3.582 477
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