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MassMS-IW-3872 N-methylbenzamide C8H9NO (Mass of molecular ion: 135)
Source Temperature: 200 °C Sample Temperature: 150 °C Reservoir, 75 eV
15.0 1.5 18.0 1.4 27.0 1.9 28.0 2.4 30.0 1.8 38.0 1.5 39.0 2.3 50.0 10.9 51.0 31.4 52.0 2.8 53.5 1.1 58.0 3.9 74.0 3.5 75.0 2.7 76.0 4.5 77.0 87.2 78.0 7.9 105.0 100.0 106.0 8.5 134.0 32.4 135.0 38.4 136.0 3.6
400 MHz in CDCl3
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1H NMR 399.65 MHz C8 H9 N O 0.042 g : 0.5 ml CDCl3 N-methylbenzamide 
Assign. Shift(ppm)
A 7.786 B 7.447 C 7.366 D 6.98 E 2.952 J(D,E)=4.8HZ
Hz ppm Int.3118.53 7.804 42 3116.58 7.799 245 3115.36 7.796 292 3114.01 7.792 143 3110.35 7.783 97 3108.28 7.778 369 3106.81 7.774 281 2986.82 7.474 39 2985.47 7.471 72 2984.25 7.468 44 2980.35 7.458 53 2978.27 7.453 185 2976.07 7.447 68 2972.17 7.437 96 2970.83 7.434 165 2969.48 7.431 88 2953.00 7.389 54 2951.17 7.385 251 2949.58 7.381 117 2944.70 7.369 205 2943.36 7.365 365 2941.89 7.362 104 2937.87 7.352 67 2936.16 7.347 157 2935.18 7.345 103 2790.16 6.982 36 1182.01 2.958 1000 1177.25 2.946 958
in CDCl3
KBr disc
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