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MS-NW-6206 2-anthrylamine C14H11N (Mass of molecular ion: 193)
Source Temperature: 160 °C Sample Temperature: 110 °C Direct, 75 eV
18.0 1.3 28.0 1.7 39.0 1.7 50.0 1.5 51.0 1.8 62.0 1.9 63.0 3.0 69.5 1.3 74.0 2.1 75.0 1.8 76.0 1.1 81.5 1.3 82.0 1.7 82.5 3.0 83.5 1.3 86.0 1.5 87.0 1.9 88.0 1.3 89.0 1.4 95.5 1.6 96.5 5.1 97.0 1.0 98.0 1.1 113.0 1.2 115.0 2.4 139.0 4.4 140.0 1.2 150.0 1.5 151.0 1.2 152.0 1.2 163.0 6.1 164.0 5.4 165.0 34.9 166.0 6.9 167.0 1.3 176.0 4.0 177.0 1.6 178.0 1.1 190.0 1.9 191.0 2.2 192.0 3.4 193.0 100.0 194.0 17.8 195.0 2.8 212.0 2.1
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C14 H11 N 0.035 g : 0.5 ml DMSO-d6 2-anthrylamine Assign. Shift(ppm)
A 8.269 B 8.037 C *1 7.901 D *1 7.866 E 7.819 F *2 7.368 G *3 7.290 J 7.091 K 6.930 L 5.60
Hz ppm Int.
3304.81 8.270 741 3212.04 8.038 747 3161.87 7.912 350 3153.44 7.891 384 3148.07 7.878 361 3143.92 7.867 34 3139.89 7.857 389 3129.64 7.831 456 3120.48 7.809 485 2953.13 7.390 183 2952.03 7.387 197 2946.66 7.374 290 2945.31 7.370 325 2943.60 7.366 192 2938.23 7.353 276 2937.01 7.349 257 2920.78 7.309 275 2919.68 7.306 290 2914.31 7.293 211 2912.60 7.288 330 2911.25 7.285 281 2905.88 7.272 198 2904.66 7.269 183 2839.48 7.105 380 2837.28 7.100 396 2830.44 7.083 366 2828.37 7.078 387 2770.63 6.933 542 2768.80 6.929 509 2238.53 5.602 1000
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