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MassMS-NW-8383 3,3'-dimethylbiphenyl C14H14 (Mass of molecular ion: 182)
Source Temperature: 260 °C Sample Temperature: 140 °C Reservoir, 75 eV
39.0 2.9 51.0 2.1 63.0 3.0 64.0 1.3 65.0 2.3 75.0 1.1 76.0 4.0 77.0 2.5 82.0 1.6 82.5 1.9 83.0 1.9 89.0 6.7 89.5 1.3 90.0 5.5 91.0 5.1 115.0 4.2 127.0 1.0 128.0 2.4 139.0 2.0 141.0 2.0 151.0 1.5 152.0 8.2 153.0 2.9 163.0 1.0 164.0 1.6 165.0 22.1 166.0 13.7 167.0 30.7 168.0 4.2 178.0 2.6 179.0 1.9 181.0 18.3 182.0 100.0 183.0 15.2 184.0 1.1
400 MHz in CDCl3
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1H NMR 399.65 MHz C14 H14 ca 10 mg : 0.5 ml CDCl3 3,3'-dimethylbiphenyl 
Assign. Shift(ppm)
A 7.364 B 7.34 C 7.255 D 7.089 E 2.353
Hz ppm Int.2945.43 7.371 135 2944.82 7.369 186 2943.73 7.366 264 2942.99 7.364 310 2942.38 7.363 267 2941.28 7.360 227 2940.55 7.358 177 2939.82 7.356 150 2939.09 7.355 148 2938.48 7.353 157 2937.87 7.352 153 2936.65 7.349 88 2936.04 7.347 72 2932.13 7.337 140 2931.52 7.336 171 2930.91 7.334 190 2930.30 7.333 206 2929.69 7.331 170 2929.08 7.330 139 2928.47 7.328 113 2906.74 7.274 185 2899.17 7.255 297 2891.36 7.235 150 2838.38 7.103 120 2837.65 7.101 153 2837.16 7.100 173 2836.55 7.098 187 2835.94 7.097 166 2835.45 7.095 149 2834.72 7.094 113 2830.93 7.084 93 2830.20 7.082 121 2829.71 7.081 135 2829.10 7.079 150 2828.49 7.078 133 2827.27 7.075 89 940.31 2.353 1000
in CDCl3
liquid film
ANION RADICAL, REDUCTION WITH K IN DME, -15C
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