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MassMS-NW-1198 N-methyl-o-toluidine C8H11N (Mass of molecular ion: 121)
Source Temperature: 240 °C Sample Temperature: 180 °C Reservoir, 75 eV
15.0 1.2 18.0 1.4 27.0 2.9 28.0 2.1 30.0 5.0 38.0 1.8 39.0 8.5 41.0 2.3 42.0 2.5 50.0 3.3 51.0 7.5 52.0 4.5 53.0 3.5 54.0 1.1 58.0 1.8 58.5 2.0 59.5 5.0 60.0 1.0 60.5 4.0 62.0 1.9 63.0 5.0 64.0 1.7 65.0 13.1 66.0 1.7 76.0 1.1 77.0 13.1 78.0 5.1 79.0 7.7 80.0 2.0 89.0 3.5 90.0 1.8 91.0 25.5 92.0 5.4 93.0 3.5 104.0 7.0 105.0 1.7 106.0 70.3 107.0 9.4 117.0 1.5 118.0 6.5 119.0 1.7 120.0 59.0 121.0 100.0 122.0 8.8 134.0 2.0 135.0 2.4
90 MHz in CDCl3
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1H NMR 89.56 MHz C8 H11 N 0.04 ml : 0.5 ml CDCl3 N-methyl-o-toluidine 
Assign. Shift(ppm)
A 7.15 B 7.03 C 6.64 D 6.60 E 3.5 F 2.862 G 2.108
Hz ppm Int.641.75 7.166 86 641.31 7.161 57 640.75 7.155 47 639.81 7.144 66 639.31 7.139 61 634.56 7.086 66 633.69 7.076 76 633.13 7.070 72 632.38 7.061 83 631.75 7.054 65 628.31 7.016 55 627.56 7.008 82 626.81 6.999 75 626.25 6.993 60 625.69 6.987 55 603.25 6.736 48 602.13 6.724 69 594.75 6.641 176 587.13 6.556 76 256.31 2.862 1000 188.75 2.108 584
in CDCl3
CCl4 solution
liquid film
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