2,4-二氯硝基苯

Mass

MS-NW-7626          
2,4-dichloro-1-nitrobenzene
C6H3Cl2NO2          (Mass of molecular ion:    191)

   Source Temperature: 250 °C
   Sample Temperature: 170 °C
   Reservoir, 75 eV

      26.0       1.1
      28.0       8.0
      30.0      44.7
      35.0       1.7
      36.0       6.8
      37.0      10.7
      38.0       6.2
      39.0       1.5
      44.0       1.3
      46.0       1.8
      47.0       2.1
      48.0       1.3
      49.0       5.9
      50.0      21.9
      51.0       3.6
      54.5       1.2
      55.0       1.0
      60.0       3.0
      61.0       6.5
      62.0       5.9
      63.0       9.2
      64.0       1.5
      71.0       1.0
      72.0       3.8
      73.0      19.2
      74.0      58.9
      75.0      46.3
      76.0       3.7
      83.0       3.8
      84.0      15.2
      85.0      12.3
      86.0       5.9
      87.0       4.6
      88.0       1.4
      97.0       3.0
      98.0       2.0
      99.0       1.2
     107.0       2.6
     108.0       3.4
     109.0     100.0
     110.0      20.9
     111.0      33.2
     112.0       6.7
     119.0       2.4
     121.0       1.6
     124.0       1.3
     126.0       1.6
     133.0      62.0
     134.0       3.8
     135.0      41.1
     136.0       2.5
     137.0       6.4
     144.0       1.7
     145.0      76.9
     146.0       6.3
     147.0      49.0
     148.0       3.7
     149.0       8.2
     161.0      62.7
     162.0       4.7
     163.0      40.8
     164.0       2.9
     165.0       6.7
     175.0       5.5
     177.0       3.8
     191.0      92.0
     192.0       7.0
     193.0      59.0
     194.0       4.6
     195.0      10.0

Assign. Shift(ppm) A 7.873 B 7.574 C 7.410 J(A,C)=8.7HZ. J(B,C)=2.2HZ.

     Hz     ppm     Int.

    710.31   7.932    566
    701.63   7.835    838
    679.56   7.588    717
    677.44   7.565   1000
    668.06   7.460    790
    665.88   7.436    573
    663.50   7.409     26
    659.38   7.363    508
    657.19   7.338    408
    655.44   7.319     28