2-溴-2,4-二甲氧基苯乙酮

产品名称 2-溴-2,4-二甲氧基苯乙酮

CAS号60965-26-6

分子式C10H11BrO3

分子量259.1

Mass

MS-NW-6977          
2-bromo-2',4'-dimethoxyacetophenone
C10H11BrO3          (Mass of molecular ion:    258)

   Source Temperature: 150 °C
   Sample Temperature: 100 °C
   Direct, 75 eV

      15.0       1.8
      18.0       2.8
      38.0       1.3
      39.0       2.7
      50.0       2.7
      51.0       5.2
      52.0       1.1
      53.0       1.6
      62.0       2.3
      63.0       5.8
      64.0       3.7
      65.0       3.4
      69.0       1.3
      74.0       1.1
      76.0       1.5
      77.0       8.1
      78.0       3.0
      79.0       2.9
      91.0       4.1
      92.0       4.6
     106.0       1.7
     107.0       3.9
     108.0       1.2
     121.0       8.6
     122.0       5.8
     135.0       2.9
     150.0       2.4
     151.0       2.6
     165.0     100.0
     166.0      10.2
     167.0       1.2
     258.0       9.4
     259.0       1.2
     260.0       9.5
     261.0       1.1

400 MHz in DMSO-d6

¹H NMR	399.65 MHz
C₁₀ H₁₁ Br O₃	0.040 g : 0.5 ml DMSO-d₆
2-bromo-2',4'-dimethoxyacetophenone

    Assign.     Shift(ppm)

      A             7.740
      B             6.682
      C             6.651
      D             4.715
      E             3.925
      F             3.864

     Hz     ppm     Int.

   3098.02   7.752    179
   3089.36   7.731    186
   2672.12   6.687    124
   2669.80   6.681    173
   2663.21   6.664    123
   2660.89   6.659     79
   2654.54   6.643    106
   2652.22   6.637     84
   1884.52   4.716    805
   1568.85   3.926    928
   1544.19   3.864   1000

KBr disc

nujol mull

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2-溴-2,4-二甲氧基苯乙酮(60965-26-6)核磁图(¹HNMR) 相关产品图谱

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