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网站主页CAS数据库列表 6088-51-3更多图谱双(6-羟基-2-萘)二硫(6088-51-3)核磁图(13CNMR)

双(6-羟基-2-萘)二硫

产品名称 双(6-羟基-2-萘)二硫

CAS号6088-51-3

分子式C20H14O2S2

分子量350.45

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  • Mass

    MS-NW-2410          
    6,6'-dithiodi-2-naphthol
    C20H14O2S2          (Mass of molecular ion:    350)
    

       Source Temperature: 230 °C
       Sample Temperature: 190 °C
       Direct, 75 eV
    

          17.0       2.3
          18.0      10.8
          28.0       3.3
          39.0       2.1
          43.0       1.0
          45.0       3.1
          50.0       1.5
          51.0       3.2
          62.0       1.8
          63.0       3.7
          65.0       1.0
          69.0       2.9
          73.0       1.0
          74.0       1.5
          75.0       2.0
          76.0       1.4
          77.0       7.1
          79.0       1.2
          87.0       2.5
          88.0       3.6
          89.0       1.8
          93.0       1.1
         102.0       7.0
         103.0       7.8
         113.0       1.4
         114.0       1.8
         115.0      30.0
         116.0       4.7
         131.0      35.2
         132.0       5.5
         143.0       2.1
         144.0      12.5
         145.0       3.5
         146.0       1.6
         147.0      12.8
         148.0       3.4
         158.0       1.5
         174.0       1.6
         175.0      46.3
         176.0     100.0
         177.0      13.1
         178.0       5.3
         286.0       1.1
         350.0      10.7
         351.0       2.6
         352.0       1.3
    

400 MHz in DMSO-d6


  • 1H NMR 399.65 MHz
    C20 H14 O2 S2 0.036 g : 0.5 ml DMSO-d6
    6,6'-dithiodi-2-naphthol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 9.97 B 7.979 C 7.744 D 7.728 E 7.537 F 7.18 G 7.14

         Hz     ppm     Int.
    

       3996.14  10.000     49
       3995.59   9.998     51
       3994.68   9.996     61
       3993.76   9.994     69
       3993.03   9.992     78
       3991.38   9.988    107
       3985.89   9.974    303
       3985.52   9.973    299
       3981.49   9.963    128
       3981.12   9.962    114
       3978.38   9.955     65
       3977.83   9.954     56
       3190.03   7.983    765
       3188.20   7.978    775
       3105.04   7.770     52
       3104.67   7.769     57
       3104.31   7.768     68
       3103.94   7.767     68
       3103.02   7.765     76
       3099.91   7.757    635
       3096.06   7.747    109
       3092.95   7.740    731
       3091.30   7.736    743
       3087.64   7.726    109
       3084.52   7.719    775
       3081.04   7.710     53
       3017.30   7.550    610
       3015.29   7.545    582
       3012.36   7.538     60
       3011.44   7.536     64
       3011.07   7.535     69
       3010.52   7.533     78
       3008.51   7.528    510
       3006.68   7.524    486
       2863.44   7.165     55
       2862.53   7.163     67
       2858.68   7.153    530
       2856.66   7.148   1000
       2854.83   7.144    866
       2852.27   7.137    306
       2850.80   7.134    107
       2849.89   7.131     86
       2849.34   7.130     85
       2846.04   7.122    604
       2843.66   7.116    433
    

in DMSO-d6



KBr disc



nujol mull