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MS-NW-2410 6,6'-dithiodi-2-naphthol C20H14O2S2 (Mass of molecular ion: 350)
Source Temperature: 230 °C Sample Temperature: 190 °C Direct, 75 eV
17.0 2.3 18.0 10.8 28.0 3.3 39.0 2.1 43.0 1.0 45.0 3.1 50.0 1.5 51.0 3.2 62.0 1.8 63.0 3.7 65.0 1.0 69.0 2.9 73.0 1.0 74.0 1.5 75.0 2.0 76.0 1.4 77.0 7.1 79.0 1.2 87.0 2.5 88.0 3.6 89.0 1.8 93.0 1.1 102.0 7.0 103.0 7.8 113.0 1.4 114.0 1.8 115.0 30.0 116.0 4.7 131.0 35.2 132.0 5.5 143.0 2.1 144.0 12.5 145.0 3.5 146.0 1.6 147.0 12.8 148.0 3.4 158.0 1.5 174.0 1.6 175.0 46.3 176.0 100.0 177.0 13.1 178.0 5.3 286.0 1.1 350.0 10.7 351.0 2.6 352.0 1.3
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C20 H14 O2 S2 0.036 g : 0.5 ml DMSO-d6 6,6'-dithiodi-2-naphthol Assign. Shift(ppm)
A 9.97 B 7.979 C 7.744 D 7.728 E 7.537 F 7.18 G 7.14
Hz ppm Int.
3996.14 10.000 49 3995.59 9.998 51 3994.68 9.996 61 3993.76 9.994 69 3993.03 9.992 78 3991.38 9.988 107 3985.89 9.974 303 3985.52 9.973 299 3981.49 9.963 128 3981.12 9.962 114 3978.38 9.955 65 3977.83 9.954 56 3190.03 7.983 765 3188.20 7.978 775 3105.04 7.770 52 3104.67 7.769 57 3104.31 7.768 68 3103.94 7.767 68 3103.02 7.765 76 3099.91 7.757 635 3096.06 7.747 109 3092.95 7.740 731 3091.30 7.736 743 3087.64 7.726 109 3084.52 7.719 775 3081.04 7.710 53 3017.30 7.550 610 3015.29 7.545 582 3012.36 7.538 60 3011.44 7.536 64 3011.07 7.535 69 3010.52 7.533 78 3008.51 7.528 510 3006.68 7.524 486 2863.44 7.165 55 2862.53 7.163 67 2858.68 7.153 530 2856.66 7.148 1000 2854.83 7.144 866 2852.27 7.137 306 2850.80 7.134 107 2849.89 7.131 86 2849.34 7.130 85 2846.04 7.122 604 2843.66 7.116 433
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